Effect of pH on Spontaneous Imbibition in Calcareous Rocks

Abstract Reactive transport in porous media exhibits multifaceted interactions that are dependent on the matrix and fluid properties, and which ultimately alter these properties. A set of calcareous rock samples with unique mineralogy and varying petrophysical properties are selected for this study....

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Main Authors: Muhammad Andiva Pratama, Hasan Javed Khan
Format: Article
Language:English
Published: Wiley 2024-04-01
Series:Water Resources Research
Subjects:
Online Access:https://doi.org/10.1029/2023WR035307
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author Muhammad Andiva Pratama
Hasan Javed Khan
author_facet Muhammad Andiva Pratama
Hasan Javed Khan
author_sort Muhammad Andiva Pratama
collection DOAJ
description Abstract Reactive transport in porous media exhibits multifaceted interactions that are dependent on the matrix and fluid properties, and which ultimately alter these properties. A set of calcareous rock samples with unique mineralogy and varying petrophysical properties are selected for this study. A capillary rise experiment is performed in each sample, first with deionized water and then with a dilute, pH 2, HCl solution. Pre‐ and post‐acid petrophysical properties such as porosity, permeability, pore size distribution, and contact angle are measured for each sample along with the capillary rise profile. The latter is tracked by applying image analysis on video recording. The rock mineralogy significantly affects the acidic fluid intrusion into the rock samples. Calcite dissolution is the main reaction that results in the opening of the pore space. This is more prominent in all the carbonate samples where a higher proportion of calcite minerals is present. A higher capillary rise is consistently observed compared to the neutral fluid along with an increase in porosity and the mean pore size. The contact angle also undergoes changes making the carbonate matrix from oil‐wet to neutral‐wet. Coupling capillary interactions with fluid reactivity is often neglected in fluid transport phenomena. This study offers new insights into the relative importance of reactivity at the timescale of spontaneous imbibition. This is important in understanding dissolution and precipitation processes during capillary flow.
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spelling doaj-art-1a21cb786b98452d96b7cdff2bc985702025-08-20T02:36:39ZengWileyWater Resources Research0043-13971944-79732024-04-01604n/an/a10.1029/2023WR035307Effect of pH on Spontaneous Imbibition in Calcareous RocksMuhammad Andiva Pratama0Hasan Javed Khan1Department of Petroleum Engineering King Fahd University of Petroleum & Minerals Dhahran Saudi ArabiaDepartment of Petroleum Engineering King Fahd University of Petroleum & Minerals Dhahran Saudi ArabiaAbstract Reactive transport in porous media exhibits multifaceted interactions that are dependent on the matrix and fluid properties, and which ultimately alter these properties. A set of calcareous rock samples with unique mineralogy and varying petrophysical properties are selected for this study. A capillary rise experiment is performed in each sample, first with deionized water and then with a dilute, pH 2, HCl solution. Pre‐ and post‐acid petrophysical properties such as porosity, permeability, pore size distribution, and contact angle are measured for each sample along with the capillary rise profile. The latter is tracked by applying image analysis on video recording. The rock mineralogy significantly affects the acidic fluid intrusion into the rock samples. Calcite dissolution is the main reaction that results in the opening of the pore space. This is more prominent in all the carbonate samples where a higher proportion of calcite minerals is present. A higher capillary rise is consistently observed compared to the neutral fluid along with an increase in porosity and the mean pore size. The contact angle also undergoes changes making the carbonate matrix from oil‐wet to neutral‐wet. Coupling capillary interactions with fluid reactivity is often neglected in fluid transport phenomena. This study offers new insights into the relative importance of reactivity at the timescale of spontaneous imbibition. This is important in understanding dissolution and precipitation processes during capillary flow.https://doi.org/10.1029/2023WR035307acidic imbibitioncalcareous rockspontaneous imbibitioncapillary rise
spellingShingle Muhammad Andiva Pratama
Hasan Javed Khan
Effect of pH on Spontaneous Imbibition in Calcareous Rocks
Water Resources Research
acidic imbibition
calcareous rock
spontaneous imbibition
capillary rise
title Effect of pH on Spontaneous Imbibition in Calcareous Rocks
title_full Effect of pH on Spontaneous Imbibition in Calcareous Rocks
title_fullStr Effect of pH on Spontaneous Imbibition in Calcareous Rocks
title_full_unstemmed Effect of pH on Spontaneous Imbibition in Calcareous Rocks
title_short Effect of pH on Spontaneous Imbibition in Calcareous Rocks
title_sort effect of ph on spontaneous imbibition in calcareous rocks
topic acidic imbibition
calcareous rock
spontaneous imbibition
capillary rise
url https://doi.org/10.1029/2023WR035307
work_keys_str_mv AT muhammadandivapratama effectofphonspontaneousimbibitionincalcareousrocks
AT hasanjavedkhan effectofphonspontaneousimbibitionincalcareousrocks