Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated Cellulose

Carbon-doped g-C3N4 was synthesized using a simple high-temperature process (calcination at 550 °C for 4 h). One-dimensional nanofibrillated cellulose (NFC) materials were then inserted into the two-dimensional g-C3N4 material by vacuum filtration method at room temperature. The prepared g-C3N4/NFC...

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Main Authors: Beiyue Xiong, Yirong Liu, Wenbiao Zheng, Xiaoxiao He, Chengning Ye, Hanyu Xue, Jianrong Xia, Renjin Gao, Liwei Wang
Format: Article
Language:English
Published: North Carolina State University 2024-11-01
Series:BioResources
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Online Access:https://ojs.bioresources.com/index.php/BRJ/article/view/24008
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author Beiyue Xiong
Yirong Liu
Wenbiao Zheng
Xiaoxiao He
Chengning Ye
Hanyu Xue
Jianrong Xia
Renjin Gao
Liwei Wang
author_facet Beiyue Xiong
Yirong Liu
Wenbiao Zheng
Xiaoxiao He
Chengning Ye
Hanyu Xue
Jianrong Xia
Renjin Gao
Liwei Wang
author_sort Beiyue Xiong
collection DOAJ
description Carbon-doped g-C3N4 was synthesized using a simple high-temperature process (calcination at 550 °C for 4 h). One-dimensional nanofibrillated cellulose (NFC) materials were then inserted into the two-dimensional g-C3N4 material by vacuum filtration method at room temperature. The prepared g-C3N4/NFC composite membranes were systematically characterized using a series of techniques, such as XRD, FTIR, and SEM. The results showed that the carbon-doped photocatalysts possessed a narrow band gap, which prolonged the visible light absorption and favored the organic pollutant degradation. The incorporation of NFC enlarged the interlayer spacing, leading to an increase in the water flux. The water flux of C0.02CN/NFC (15%) composite membranes reached 73.7 L•m-2•h-1•bar-1, which is more than that of g-C3N4/NFC membrane. At the same time, the carbon doped composite membranes showed enhanced retention and photocatalytic degradation ability. The retention rate of the C0.02CN/NFC (5%) composite membranes could reach 89.3% from 80.8% after three-cycle photocatalytic experiments. The membrane maintained a good retention rate and feed flux, which confirms the composite membrane has good self-cleaning ability and stability. It could potentially be applied for water treatment.
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id doaj-art-16c5fb2833cc49afaf938dc0c3a2991f
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issn 1930-2126
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publishDate 2024-11-01
publisher North Carolina State University
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spelling doaj-art-16c5fb2833cc49afaf938dc0c3a2991f2025-08-20T02:56:43ZengNorth Carolina State UniversityBioResources1930-21262024-11-012018098252235Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated CelluloseBeiyue Xiong0Yirong Liu1Wenbiao Zheng2Xiaoxiao He3Chengning Ye4Hanyu Xue5https://orcid.org/0000-0001-9160-2290Jianrong Xia6https://orcid.org/0000-0001-5871-6309Renjin Gao7Liwei Wang8https://orcid.org/0000-0002-0741-157XCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, ChinaCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, ChinaCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, China; College of Environment and Safety Engineering, Fuzhou University, Fuzhou 350116, ChinaCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, ChinaCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, China; College of Materials Engineering, Fujian Agriculture and Forestry University, Fuzhou 350002College of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, ChinaCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, ChinaCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, ChinaCollege of Materials and Chemical Engineering, Minjiang University, Fuzhou 350108, ChinaCarbon-doped g-C3N4 was synthesized using a simple high-temperature process (calcination at 550 °C for 4 h). One-dimensional nanofibrillated cellulose (NFC) materials were then inserted into the two-dimensional g-C3N4 material by vacuum filtration method at room temperature. The prepared g-C3N4/NFC composite membranes were systematically characterized using a series of techniques, such as XRD, FTIR, and SEM. The results showed that the carbon-doped photocatalysts possessed a narrow band gap, which prolonged the visible light absorption and favored the organic pollutant degradation. The incorporation of NFC enlarged the interlayer spacing, leading to an increase in the water flux. The water flux of C0.02CN/NFC (15%) composite membranes reached 73.7 L•m-2•h-1•bar-1, which is more than that of g-C3N4/NFC membrane. At the same time, the carbon doped composite membranes showed enhanced retention and photocatalytic degradation ability. The retention rate of the C0.02CN/NFC (5%) composite membranes could reach 89.3% from 80.8% after three-cycle photocatalytic experiments. The membrane maintained a good retention rate and feed flux, which confirms the composite membrane has good self-cleaning ability and stability. It could potentially be applied for water treatment.https://ojs.bioresources.com/index.php/BRJ/article/view/24008graphitic phase carbon nitridephotocatalysiscomposite membranecellulose water flux
spellingShingle Beiyue Xiong
Yirong Liu
Wenbiao Zheng
Xiaoxiao He
Chengning Ye
Hanyu Xue
Jianrong Xia
Renjin Gao
Liwei Wang
Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated Cellulose
BioResources
graphitic phase carbon nitride
photocatalysis
composite membrane
cellulose
water flux
title Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated Cellulose
title_full Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated Cellulose
title_fullStr Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated Cellulose
title_full_unstemmed Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated Cellulose
title_short Enhanced Photocatalytic and Filtration Properties of Carbon-Doped g-C3N4 Membranes Reinforced with Nanofibrillated Cellulose
title_sort enhanced photocatalytic and filtration properties of carbon doped g c3n4 membranes reinforced with nanofibrillated cellulose
topic graphitic phase carbon nitride
photocatalysis
composite membrane
cellulose
water flux
url https://ojs.bioresources.com/index.php/BRJ/article/view/24008
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