Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory Method

A systematic vibrational spectroscopic assignment and analysis of tenofovir has been carried out by using FTIR and FT-Raman spectral data. The vibrational analysis was aided by electronic structure calculations—hybrid density functional methods (B3LYP/6-311++G(d,p), B3LYP/6-31G(d,p), and B3PW91/6-31...

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Main Authors: G. R. Ramkumaar, S. Srinivasan, T. J. Bhoopathy, S. Gunasekaran
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2013/126502
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author G. R. Ramkumaar
S. Srinivasan
T. J. Bhoopathy
S. Gunasekaran
author_facet G. R. Ramkumaar
S. Srinivasan
T. J. Bhoopathy
S. Gunasekaran
author_sort G. R. Ramkumaar
collection DOAJ
description A systematic vibrational spectroscopic assignment and analysis of tenofovir has been carried out by using FTIR and FT-Raman spectral data. The vibrational analysis was aided by electronic structure calculations—hybrid density functional methods (B3LYP/6-311++G(d,p), B3LYP/6-31G(d,p), and B3PW91/6-31G(d,p). Molecular equilibrium geometries, electronic energies, IR intensities, and harmonic vibrational frequencies have been computed. The assignments proposed based on the experimental IR and Raman spectra have been reviewed and complete assignment of the observed spectra have been proposed. UV-visible spectrum of the compound was also recorded and the electronic properties such as HOMO and LUMO energies and were determined by time-dependent DFT (TD-DFT) method. The geometrical, thermodynamical parameters, and absorption wavelengths were compared with the experimental data. The B3LYP/6-311++G(d,p)-, B3LYP/6-31G(d,p)-, and B3PW91/6-31G(d,p)-based NMR calculation procedure was also done. It was used to assign the 13C and 1H NMR chemical shift of tenofovir.
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spelling doaj-art-13d7b3c19c49412dae2eaaa9900e0f312025-08-20T02:01:42ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/126502126502Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory MethodG. R. Ramkumaar0S. Srinivasan1T. J. Bhoopathy2S. Gunasekaran3PG and Research Department of Physics, Pachaiyappa's College, Chennai 600030, IndiaPG and Research Department of Physics, Presidency College, Chennai 600005, IndiaPG and Research Department of Physics, Pachaiyappa's College, Chennai 600030, IndiaPG and Research Department of Physics, Pachaiyappa's College, Chennai 600030, IndiaA systematic vibrational spectroscopic assignment and analysis of tenofovir has been carried out by using FTIR and FT-Raman spectral data. The vibrational analysis was aided by electronic structure calculations—hybrid density functional methods (B3LYP/6-311++G(d,p), B3LYP/6-31G(d,p), and B3PW91/6-31G(d,p). Molecular equilibrium geometries, electronic energies, IR intensities, and harmonic vibrational frequencies have been computed. The assignments proposed based on the experimental IR and Raman spectra have been reviewed and complete assignment of the observed spectra have been proposed. UV-visible spectrum of the compound was also recorded and the electronic properties such as HOMO and LUMO energies and were determined by time-dependent DFT (TD-DFT) method. The geometrical, thermodynamical parameters, and absorption wavelengths were compared with the experimental data. The B3LYP/6-311++G(d,p)-, B3LYP/6-31G(d,p)-, and B3PW91/6-31G(d,p)-based NMR calculation procedure was also done. It was used to assign the 13C and 1H NMR chemical shift of tenofovir.http://dx.doi.org/10.1155/2013/126502
spellingShingle G. R. Ramkumaar
S. Srinivasan
T. J. Bhoopathy
S. Gunasekaran
Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory Method
Journal of Chemistry
title Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory Method
title_full Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory Method
title_fullStr Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory Method
title_full_unstemmed Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory Method
title_short Vibrational Spectroscopic Studies of Tenofovir Using Density Functional Theory Method
title_sort vibrational spectroscopic studies of tenofovir using density functional theory method
url http://dx.doi.org/10.1155/2013/126502
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AT ssrinivasan vibrationalspectroscopicstudiesoftenofovirusingdensityfunctionaltheorymethod
AT tjbhoopathy vibrationalspectroscopicstudiesoftenofovirusingdensityfunctionaltheorymethod
AT sgunasekaran vibrationalspectroscopicstudiesoftenofovirusingdensityfunctionaltheorymethod