Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning Materials
Fe:TiO2 nano particles were deposited through sol-gel techniques, and the influence of pH values on structural, morphological, optical, and photoluminescence spectral behaviors was studied. Iron doped titanium dioxide nanopowders were analyzed using XRD, SEM, UV–ViS, and PL. Nano crystallized sample...
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Wiley
2022-01-01
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| Series: | Advances in Materials Science and Engineering |
| Online Access: | http://dx.doi.org/10.1155/2022/2748908 |
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| author | Tizazu Abza Abel Saka Jule Leta Tesfaye Lamessa Gudata N. Nagaprasad Ramaswamy Krishnaraj |
| author_facet | Tizazu Abza Abel Saka Jule Leta Tesfaye Lamessa Gudata N. Nagaprasad Ramaswamy Krishnaraj |
| author_sort | Tizazu Abza |
| collection | DOAJ |
| description | Fe:TiO2 nano particles were deposited through sol-gel techniques, and the influence of pH values on structural, morphological, optical, and photoluminescence spectral behaviors was studied. Iron doped titanium dioxide nanopowders were analyzed using XRD, SEM, UV–ViS, and PL. Nano crystallized samples of titanium dioxide (72 nm, 77 nm, 78 nm, and 83 nm) were gained from X-Ray diffraction data and showed that there was the creation of unalloyed anatase and ructile segment with tetragonal configuration. The average crystal size was 77.5 nm. pH values provide the alteration of segments from anatase to ructile. The crystal size of prepared iron doped titanium dioxide nanoparticles was greater than before as pH value rises from 2 to 6 while FWHM and scrap sizes declined. Homogeneously disseminated cylindrical forms of iron doped titanium dioxide nanoparticles were perceived from scanning electron microscope graphics and rises in size with growing pH values from 2 to 6 in an acidic medium. Extremely translucent nanopowders are witnessed in the observable region by visible and redshifts near advanced wavelengths with rising pH values because of an increase in the size of particles from XRD data and SEM micrographs. The band gap of energy produced by nano concentrates was reduced with growing pH values that resemble the redshift of optical absorption superiority. The structural behaviors of deposited nanoparticles were also analyzed by Raman spectra and disclosed the existence of tetragonal anatase and ructile segments. EDS results confirmed that the dopant of pH values of the solutions might affect the size distributions of the Fe: TiO2 nanoparticles. The general decrement intensity was witnessed from photoluminescence outcomes. |
| format | Article |
| id | doaj-art-1365a4c8582345719ed26a432e51afa1 |
| institution | Kabale University |
| issn | 1687-8442 |
| language | English |
| publishDate | 2022-01-01 |
| publisher | Wiley |
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| series | Advances in Materials Science and Engineering |
| spelling | doaj-art-1365a4c8582345719ed26a432e51afa12025-02-03T05:51:01ZengWileyAdvances in Materials Science and Engineering1687-84422022-01-01202210.1155/2022/2748908Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning MaterialsTizazu Abza0Abel Saka1Jule Leta Tesfaye2Lamessa Gudata3N. Nagaprasad4Ramaswamy Krishnaraj5Hawassa UniversityDambi Dollo UniversityDambi Dollo UniversityDambi Dollo UniversityDepartment of Mechanical EngineeringCentre for Excellence-Indigenous KnowledgeFe:TiO2 nano particles were deposited through sol-gel techniques, and the influence of pH values on structural, morphological, optical, and photoluminescence spectral behaviors was studied. Iron doped titanium dioxide nanopowders were analyzed using XRD, SEM, UV–ViS, and PL. Nano crystallized samples of titanium dioxide (72 nm, 77 nm, 78 nm, and 83 nm) were gained from X-Ray diffraction data and showed that there was the creation of unalloyed anatase and ructile segment with tetragonal configuration. The average crystal size was 77.5 nm. pH values provide the alteration of segments from anatase to ructile. The crystal size of prepared iron doped titanium dioxide nanoparticles was greater than before as pH value rises from 2 to 6 while FWHM and scrap sizes declined. Homogeneously disseminated cylindrical forms of iron doped titanium dioxide nanoparticles were perceived from scanning electron microscope graphics and rises in size with growing pH values from 2 to 6 in an acidic medium. Extremely translucent nanopowders are witnessed in the observable region by visible and redshifts near advanced wavelengths with rising pH values because of an increase in the size of particles from XRD data and SEM micrographs. The band gap of energy produced by nano concentrates was reduced with growing pH values that resemble the redshift of optical absorption superiority. The structural behaviors of deposited nanoparticles were also analyzed by Raman spectra and disclosed the existence of tetragonal anatase and ructile segments. EDS results confirmed that the dopant of pH values of the solutions might affect the size distributions of the Fe: TiO2 nanoparticles. The general decrement intensity was witnessed from photoluminescence outcomes.http://dx.doi.org/10.1155/2022/2748908 |
| spellingShingle | Tizazu Abza Abel Saka Jule Leta Tesfaye Lamessa Gudata N. Nagaprasad Ramaswamy Krishnaraj Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning Materials Advances in Materials Science and Engineering |
| title | Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning Materials |
| title_full | Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning Materials |
| title_fullStr | Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning Materials |
| title_full_unstemmed | Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning Materials |
| title_short | Synthesis and Characterization of Iron Doped Titanium Dioxide (Fe: TiO2) Nanoprecipitate at Different pH Values for Applications of Self-Cleaning Materials |
| title_sort | synthesis and characterization of iron doped titanium dioxide fe tio2 nanoprecipitate at different ph values for applications of self cleaning materials |
| url | http://dx.doi.org/10.1155/2022/2748908 |
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