Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion Batteries

Abstract Aluminum metal is a promising material for aluminum‐ion battery (AIB) anodes due to its sustainable cycle life. However, retaining the stability of aluminum anodes remains a challenge, particularly due to complex interfacial reactions with ionic liquid electrolytes. This study examines the...

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Main Authors: Nattha Chaiyapo, Yujeong Jeong, Sujeera Plueksachard, Pornjira Phuenhinlad, Panya Thanwisai, Jeffrey Nash, Wanwisa Limphirat, Jayaraman Theerthagiri, Myong Yong Choi, Nonglak Meethong
Format: Article
Language:English
Published: Wiley-VCH 2025-08-01
Series:Advanced Materials Interfaces
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Online Access:https://doi.org/10.1002/admi.202500289
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author Nattha Chaiyapo
Yujeong Jeong
Sujeera Plueksachard
Pornjira Phuenhinlad
Panya Thanwisai
Jeffrey Nash
Wanwisa Limphirat
Jayaraman Theerthagiri
Myong Yong Choi
Nonglak Meethong
author_facet Nattha Chaiyapo
Yujeong Jeong
Sujeera Plueksachard
Pornjira Phuenhinlad
Panya Thanwisai
Jeffrey Nash
Wanwisa Limphirat
Jayaraman Theerthagiri
Myong Yong Choi
Nonglak Meethong
author_sort Nattha Chaiyapo
collection DOAJ
description Abstract Aluminum metal is a promising material for aluminum‐ion battery (AIB) anodes due to its sustainable cycle life. However, retaining the stability of aluminum anodes remains a challenge, particularly due to complex interfacial reactions with ionic liquid electrolytes. This study examines the behavior of aluminum foil anodes in varying molar ratios of AlCl3:EMIC ionic liquid electrolytes. Study results reveal that the electrolytes cause damage to the native oxide layer of aluminum foils, leading to their transformation into amorphous aluminum oxide. This is confirmed using Al K‐edge X‐ray absorption spectroscopy (XAS) and X‐ray photoelectron spectroscopy (XPS). In contrast, basic electrolytes promote the deposition of an oxidized layer incorporating anions, which increases interfacial resistance with dendrite formation. These findings highlight the critical role of electrolyte composition in determining surface reactions and stability. This work provides novel insights into the interfacial mechanisms governing aluminum anodes and serves as a guideline for designing stable, non‐aqueous AIB systems.
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issn 2196-7350
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series Advanced Materials Interfaces
spelling doaj-art-1245c5ae8eae4c1b83f8bfdcfaa959852025-08-20T02:55:05ZengWiley-VCHAdvanced Materials Interfaces2196-73502025-08-011215n/an/a10.1002/admi.202500289Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion BatteriesNattha Chaiyapo0Yujeong Jeong1Sujeera Plueksachard2Pornjira Phuenhinlad3Panya Thanwisai4Jeffrey Nash5Wanwisa Limphirat6Jayaraman Theerthagiri7Myong Yong Choi8Nonglak Meethong9Department of Physics Faculty of Science Khon Kaen University Khon Kaen 40002 ThailandCore‐Facility Center for Photochemistry & Nanomaterials Department of Chemistry (BK21 FOUR) Research Institute of Natural Sciences Gyeongsang National University Jinju 52828 Republic of KoreaDepartment of Physics Faculty of Science Khon Kaen University Khon Kaen 40002 ThailandInstitute of Nanomaterials Research and Innovation for Energy (IN‐RIE) Faculty of Science Khon Kaen University Khon Kaen 40002 ThailandDepartment of Mechanical and Materials Engineering Worcester Polytechnic Institute Worcester MA 01609 USAInstitute of Nanomaterials Research and Innovation for Energy (IN‐RIE) Faculty of Science Khon Kaen University Khon Kaen 40002 ThailandSynchrotron Light Research Institute (Public Organization) Nakhon Ratchasima 30000 ThailandCore‐Facility Center for Photochemistry & Nanomaterials Department of Chemistry (BK21 FOUR) Research Institute of Natural Sciences Gyeongsang National University Jinju 52828 Republic of KoreaCore‐Facility Center for Photochemistry & Nanomaterials Department of Chemistry (BK21 FOUR) Research Institute of Natural Sciences Gyeongsang National University Jinju 52828 Republic of KoreaDepartment of Physics Faculty of Science Khon Kaen University Khon Kaen 40002 ThailandAbstract Aluminum metal is a promising material for aluminum‐ion battery (AIB) anodes due to its sustainable cycle life. However, retaining the stability of aluminum anodes remains a challenge, particularly due to complex interfacial reactions with ionic liquid electrolytes. This study examines the behavior of aluminum foil anodes in varying molar ratios of AlCl3:EMIC ionic liquid electrolytes. Study results reveal that the electrolytes cause damage to the native oxide layer of aluminum foils, leading to their transformation into amorphous aluminum oxide. This is confirmed using Al K‐edge X‐ray absorption spectroscopy (XAS) and X‐ray photoelectron spectroscopy (XPS). In contrast, basic electrolytes promote the deposition of an oxidized layer incorporating anions, which increases interfacial resistance with dendrite formation. These findings highlight the critical role of electrolyte composition in determining surface reactions and stability. This work provides novel insights into the interfacial mechanisms governing aluminum anodes and serves as a guideline for designing stable, non‐aqueous AIB systems.https://doi.org/10.1002/admi.202500289aluminum‐ion batteriesaluminum metalanode materialsionic liquid electrolytesolid electrolyte interface
spellingShingle Nattha Chaiyapo
Yujeong Jeong
Sujeera Plueksachard
Pornjira Phuenhinlad
Panya Thanwisai
Jeffrey Nash
Wanwisa Limphirat
Jayaraman Theerthagiri
Myong Yong Choi
Nonglak Meethong
Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion Batteries
Advanced Materials Interfaces
aluminum‐ion batteries
aluminum metal
anode materials
ionic liquid electrolyte
solid electrolyte interface
title Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion Batteries
title_full Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion Batteries
title_fullStr Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion Batteries
title_full_unstemmed Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion Batteries
title_short Impact of Electrolyte Concentration on Surface Properties and Electrochemical Performance of Aluminum Anodes in Aluminum‐Ion Batteries
title_sort impact of electrolyte concentration on surface properties and electrochemical performance of aluminum anodes in aluminum ion batteries
topic aluminum‐ion batteries
aluminum metal
anode materials
ionic liquid electrolyte
solid electrolyte interface
url https://doi.org/10.1002/admi.202500289
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