Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel Cells

Optimizing fuel cells for hot and dry conditions is crucial for heavy‐duty vehicle applications. This study focuses on enhancing gas diffusion layers (GDLs) to improve water management and performance of hydrocarbon (HC) catalyst‐coated membranes (CCMs). Thirty‐micrometer thin, self‐standing, and fl...

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Main Authors: Koray Yildirim, Florian Lombeck, Severin Vierrath, Matthias Breitwieser
Format: Article
Language:English
Published: Wiley-VCH 2025-08-01
Series:Advanced Energy & Sustainability Research
Subjects:
Online Access:https://doi.org/10.1002/aesr.202400429
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author Koray Yildirim
Florian Lombeck
Severin Vierrath
Matthias Breitwieser
author_facet Koray Yildirim
Florian Lombeck
Severin Vierrath
Matthias Breitwieser
author_sort Koray Yildirim
collection DOAJ
description Optimizing fuel cells for hot and dry conditions is crucial for heavy‐duty vehicle applications. This study focuses on enhancing gas diffusion layers (GDLs) to improve water management and performance of hydrocarbon (HC) catalyst‐coated membranes (CCMs). Thirty‐micrometer thin, self‐standing, and fluorine‐free microporous layers (SS‐MPLs) for fuel cell anodes using carbon black, graphite, and acrylic binder are developed. The impact of carbon black and binder quantities in SS‐MPL compositions on morphology, surface wetting, permeability, electrical resistance, and electrochemical performance is investigated. The SS‐MPLs demonstrate more homogeneous morphology and ≈10 times lower permeability compared to commercial references. Increasing carbon black in the SS‐MPLs reduces permeability by a factor of ≈5. Contact angle measurements indicate a hydrophilic nature for all SS‐MPLs, which is beneficial for water retention in hot and dry conditions. Optimal composition of 30% binder and 25% carbon black for the MPL, enabled a 41% higher current density (1243 mA cm−2) compared to the commercial anode GDL reference H14Cx653 (881 mA cm−2) at 0.65 V in 105 °C under 35 and 60% relative humidity at the anode and cathode. These results highlight the importance of GDLs in future membrane electrode assembly designs, particularly for HC‐based CCMs, which are more sensitive to humidity.
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institution Kabale University
issn 2699-9412
language English
publishDate 2025-08-01
publisher Wiley-VCH
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series Advanced Energy & Sustainability Research
spelling doaj-art-11d1391d52964f0b9f9cd687bc03100a2025-08-20T04:02:12ZengWiley-VCHAdvanced Energy & Sustainability Research2699-94122025-08-0168n/an/a10.1002/aesr.202400429Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel CellsKoray Yildirim0Florian Lombeck1Severin Vierrath2Matthias Breitwieser3Electrochemical Energy Systems, IMTEK – Department of Microsystems Engineering University of Freiburg Georges‐Koehler‐Allee 103 79110 Freiburg Germanyionysis GmbH Georges‐Koehler‐Allee 103 79110 Freiburg GermanyElectrochemical Energy Systems, IMTEK – Department of Microsystems Engineering University of Freiburg Georges‐Koehler‐Allee 103 79110 Freiburg GermanyElectrochemical Energy Systems, IMTEK – Department of Microsystems Engineering University of Freiburg Georges‐Koehler‐Allee 103 79110 Freiburg GermanyOptimizing fuel cells for hot and dry conditions is crucial for heavy‐duty vehicle applications. This study focuses on enhancing gas diffusion layers (GDLs) to improve water management and performance of hydrocarbon (HC) catalyst‐coated membranes (CCMs). Thirty‐micrometer thin, self‐standing, and fluorine‐free microporous layers (SS‐MPLs) for fuel cell anodes using carbon black, graphite, and acrylic binder are developed. The impact of carbon black and binder quantities in SS‐MPL compositions on morphology, surface wetting, permeability, electrical resistance, and electrochemical performance is investigated. The SS‐MPLs demonstrate more homogeneous morphology and ≈10 times lower permeability compared to commercial references. Increasing carbon black in the SS‐MPLs reduces permeability by a factor of ≈5. Contact angle measurements indicate a hydrophilic nature for all SS‐MPLs, which is beneficial for water retention in hot and dry conditions. Optimal composition of 30% binder and 25% carbon black for the MPL, enabled a 41% higher current density (1243 mA cm−2) compared to the commercial anode GDL reference H14Cx653 (881 mA cm−2) at 0.65 V in 105 °C under 35 and 60% relative humidity at the anode and cathode. These results highlight the importance of GDLs in future membrane electrode assembly designs, particularly for HC‐based CCMs, which are more sensitive to humidity.https://doi.org/10.1002/aesr.202400429fluorine‐free fuel cellshot and dry operating conditionsself‐standing microporous layerswater management
spellingShingle Koray Yildirim
Florian Lombeck
Severin Vierrath
Matthias Breitwieser
Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel Cells
Advanced Energy & Sustainability Research
fluorine‐free fuel cells
hot and dry operating conditions
self‐standing microporous layers
water management
title Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel Cells
title_full Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel Cells
title_fullStr Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel Cells
title_full_unstemmed Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel Cells
title_short Self‐Standing Fluorine‐Free Anode Microporous Layers Enabling Improved Hot and Dry Operation of Fully Hydrocarbon Proton‐Exchange Membrane Fuel Cells
title_sort self standing fluorine free anode microporous layers enabling improved hot and dry operation of fully hydrocarbon proton exchange membrane fuel cells
topic fluorine‐free fuel cells
hot and dry operating conditions
self‐standing microporous layers
water management
url https://doi.org/10.1002/aesr.202400429
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AT florianlombeck selfstandingfluorinefreeanodemicroporouslayersenablingimprovedhotanddryoperationoffullyhydrocarbonprotonexchangemembranefuelcells
AT severinvierrath selfstandingfluorinefreeanodemicroporouslayersenablingimprovedhotanddryoperationoffullyhydrocarbonprotonexchangemembranefuelcells
AT matthiasbreitwieser selfstandingfluorinefreeanodemicroporouslayersenablingimprovedhotanddryoperationoffullyhydrocarbonprotonexchangemembranefuelcells