Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticles

Composites of natural rubber (NR)/vinyl polymer nanoparticles as polystyrene (PS) and poly(styrenemethacrylic acid) (P(S-MAA)) were prepared by heterocoagulation technique. The polymer nanoparticles were prepared by emulsifier-free emulsion polymerizations at 70°C using potassium persulfate as initi...

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Main Authors: T. Nuruk, C. Suksawad, A. Chaiyasat, P. Chaiyasat
Format: Article
Language:English
Published: Budapest University of Technology and Economics 2012-06-01
Series:eXPRESS Polymer Letters
Subjects:
Online Access:http://www.expresspolymlett.com/letolt.php?file=EPL-0003170&mi=cd
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author T. Nuruk
C. Suksawad
A. Chaiyasat
P. Chaiyasat
author_facet T. Nuruk
C. Suksawad
A. Chaiyasat
P. Chaiyasat
author_sort T. Nuruk
collection DOAJ
description Composites of natural rubber (NR)/vinyl polymer nanoparticles as polystyrene (PS) and poly(styrenemethacrylic acid) (P(S-MAA)) were prepared by heterocoagulation technique. The polymer nanoparticles were prepared by emulsifier-free emulsion polymerizations at 70°C using potassium persulfate as initiator. Under acidic condition where positive charge was present on the NR latex (NRL) surface, the nanoparticles having negative charge mainly from sulfate group of initiator were able to adsorb on the NRL surface, the electrostatic interaction being the driving force. The scanning electron micrographs showed that the polymer nanoparticles are homogenously distributed throughout NR matrix as nanoclusters with an average size of about 500 and 200 nm for PS and P(S-MAA), respectively. The mechanical properties of NR/PS and NR/P(S-MAA) composite films were compared with the NR host. The nanocomposites, particularly when the polymer nanoparticles are uniformly dispersed, possess significantly enhanced mechanical properties strongly depending on the morphology of the nanocomposites.
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institution Kabale University
issn 1788-618X
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publishDate 2012-06-01
publisher Budapest University of Technology and Economics
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series eXPRESS Polymer Letters
spelling doaj-art-110f740561cf4b93bcfbe00b4f064b642025-08-20T03:33:26ZengBudapest University of Technology and EconomicseXPRESS Polymer Letters1788-618X2012-06-016651151810.3144/expresspolymlett.2012.54Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticlesT. NurukC. SuksawadA. ChaiyasatP. ChaiyasatComposites of natural rubber (NR)/vinyl polymer nanoparticles as polystyrene (PS) and poly(styrenemethacrylic acid) (P(S-MAA)) were prepared by heterocoagulation technique. The polymer nanoparticles were prepared by emulsifier-free emulsion polymerizations at 70°C using potassium persulfate as initiator. Under acidic condition where positive charge was present on the NR latex (NRL) surface, the nanoparticles having negative charge mainly from sulfate group of initiator were able to adsorb on the NRL surface, the electrostatic interaction being the driving force. The scanning electron micrographs showed that the polymer nanoparticles are homogenously distributed throughout NR matrix as nanoclusters with an average size of about 500 and 200 nm for PS and P(S-MAA), respectively. The mechanical properties of NR/PS and NR/P(S-MAA) composite films were compared with the NR host. The nanocomposites, particularly when the polymer nanoparticles are uniformly dispersed, possess significantly enhanced mechanical properties strongly depending on the morphology of the nanocomposites.http://www.expresspolymlett.com/letolt.php?file=EPL-0003170&mi=cdNanocompositesheterocoagulationnatural rubber latex
spellingShingle T. Nuruk
C. Suksawad
A. Chaiyasat
P. Chaiyasat
Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticles
eXPRESS Polymer Letters
Nanocomposites
heterocoagulation
natural rubber latex
title Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticles
title_full Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticles
title_fullStr Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticles
title_full_unstemmed Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticles
title_short Preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene-methacrylic acid copolymer nanoparticles
title_sort preparation and characterization of nanocomposites of natural rubber with polystyrene and styrene methacrylic acid copolymer nanoparticles
topic Nanocomposites
heterocoagulation
natural rubber latex
url http://www.expresspolymlett.com/letolt.php?file=EPL-0003170&mi=cd
work_keys_str_mv AT tnuruk preparationandcharacterizationofnanocompositesofnaturalrubberwithpolystyreneandstyrenemethacrylicacidcopolymernanoparticles
AT csuksawad preparationandcharacterizationofnanocompositesofnaturalrubberwithpolystyreneandstyrenemethacrylicacidcopolymernanoparticles
AT achaiyasat preparationandcharacterizationofnanocompositesofnaturalrubberwithpolystyreneandstyrenemethacrylicacidcopolymernanoparticles
AT pchaiyasat preparationandcharacterizationofnanocompositesofnaturalrubberwithpolystyreneandstyrenemethacrylicacidcopolymernanoparticles