Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed Fluoridation

Sulfur hexafluoride (SF<sub>6</sub>), the strongest greenhouse gas, has great challenges in degradation because of its stable structure, posing significant environmental concerns. Photocatalysis offers an environmentally friendly, low-energy solution, but the fluoride deposition on catal...

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Main Authors: Wenhui Zhou, Boxu Dong, Ziqi Si, Yushuai Xu, Xinhua He, Ziyi Zhan, Yaru Zhang, Chaoyu Song, Zhuoqian Lv, Jiantao Zai, Xuefeng Qian
Format: Article
Language:English
Published: MDPI AG 2025-03-01
Series:Molecules
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Online Access:https://www.mdpi.com/1420-3049/30/7/1481
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author Wenhui Zhou
Boxu Dong
Ziqi Si
Yushuai Xu
Xinhua He
Ziyi Zhan
Yaru Zhang
Chaoyu Song
Zhuoqian Lv
Jiantao Zai
Xuefeng Qian
author_facet Wenhui Zhou
Boxu Dong
Ziqi Si
Yushuai Xu
Xinhua He
Ziyi Zhan
Yaru Zhang
Chaoyu Song
Zhuoqian Lv
Jiantao Zai
Xuefeng Qian
author_sort Wenhui Zhou
collection DOAJ
description Sulfur hexafluoride (SF<sub>6</sub>), the strongest greenhouse gas, has great challenges in degradation because of its stable structure, posing significant environmental concerns. Photocatalysis offers an environmentally friendly, low-energy solution, but the fluoride deposition on catalysts reduces their activity, thus limiting their large-scale application. To prevent catalyst fluoride poisoning, we report a thin-layer graphitic carbon nitride (CN) material loaded with MoO<sub>x</sub> (CNM) that resists fluoride deposition for long-term SF<sub>6</sub> degradation. By combining molecular structure design and nanostructure regulation, we construct a photocatalyst with enhanced charge carrier mobility and reduced transport distances. We find that the CNM exhibits a high specific surface area, increased contact between reactants and active sites, and efficient electron–hole separation due to the Mo-N bonds, achieving an SF<sub>6</sub> degradation efficiency of 1.73 mmol/g after one day due to the prolonged catalytic durability of the catalyst, which is eight times higher than pristine g-C<sub>3</sub>N<sub>4</sub> (0.21 mmol/g). We demonstrate the potential of CNMs for low-energy, high-efficiency SF<sub>6</sub> degradation, offering a new approach to mitigate the environmental impact of this potent greenhouse gas. We envision that this study will inspire further research into advanced photocatalytic materials for environmental remediation, contributing to global efforts in combating climate change.
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publishDate 2025-03-01
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spelling doaj-art-10b26f5e8c5a4d42a3ba823ea3e7b7302025-08-20T03:08:55ZengMDPI AGMolecules1420-30492025-03-01307148110.3390/molecules30071481Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed FluoridationWenhui Zhou0Boxu Dong1Ziqi Si2Yushuai Xu3Xinhua He4Ziyi Zhan5Yaru Zhang6Chaoyu Song7Zhuoqian Lv8Jiantao Zai9Xuefeng Qian10Shaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaShaoxing Research Institute of Renewable Energy and Molecular Engineering, School of Chemistry and Chemical Engineering, Shanghai Jiao Tong University, Shanghai 200240, ChinaSulfur hexafluoride (SF<sub>6</sub>), the strongest greenhouse gas, has great challenges in degradation because of its stable structure, posing significant environmental concerns. Photocatalysis offers an environmentally friendly, low-energy solution, but the fluoride deposition on catalysts reduces their activity, thus limiting their large-scale application. To prevent catalyst fluoride poisoning, we report a thin-layer graphitic carbon nitride (CN) material loaded with MoO<sub>x</sub> (CNM) that resists fluoride deposition for long-term SF<sub>6</sub> degradation. By combining molecular structure design and nanostructure regulation, we construct a photocatalyst with enhanced charge carrier mobility and reduced transport distances. We find that the CNM exhibits a high specific surface area, increased contact between reactants and active sites, and efficient electron–hole separation due to the Mo-N bonds, achieving an SF<sub>6</sub> degradation efficiency of 1.73 mmol/g after one day due to the prolonged catalytic durability of the catalyst, which is eight times higher than pristine g-C<sub>3</sub>N<sub>4</sub> (0.21 mmol/g). We demonstrate the potential of CNMs for low-energy, high-efficiency SF<sub>6</sub> degradation, offering a new approach to mitigate the environmental impact of this potent greenhouse gas. We envision that this study will inspire further research into advanced photocatalytic materials for environmental remediation, contributing to global efforts in combating climate change.https://www.mdpi.com/1420-3049/30/7/1481photocatalysissulfur hexafluoride degradationstabilityheterostructures
spellingShingle Wenhui Zhou
Boxu Dong
Ziqi Si
Yushuai Xu
Xinhua He
Ziyi Zhan
Yaru Zhang
Chaoyu Song
Zhuoqian Lv
Jiantao Zai
Xuefeng Qian
Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed Fluoridation
Molecules
photocatalysis
sulfur hexafluoride degradation
stability
heterostructures
title Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed Fluoridation
title_full Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed Fluoridation
title_fullStr Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed Fluoridation
title_full_unstemmed Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed Fluoridation
title_short Surface-Engineered MoO<sub>x</sub>/CN Heterostructures Enable Long-Term SF<sub>6</sub> Photodegradation via Suppressed Fluoridation
title_sort surface engineered moo sub x sub cn heterostructures enable long term sf sub 6 sub photodegradation via suppressed fluoridation
topic photocatalysis
sulfur hexafluoride degradation
stability
heterostructures
url https://www.mdpi.com/1420-3049/30/7/1481
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