Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion Film

Electrodeposited gold and Nafion-gold composite on the surface of glassy carbon electrodes (GCE) have shown electrocatalytic activity during guanine oxidation. In comparison with the unmodified electrode, decreasing of the oxidation potential by 100 mV and increasing of the current of organic compou...

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Main Authors: L.G. Shaidarova, A.V. Gedmina, V.D. Demina, I.A. Chelnokova, H.C. Budnikov
Format: Article
Language:English
Published: Kazan Federal University 2016-09-01
Series:Учёные записки Казанского университета: Серия Естественные науки
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Online Access:http://kpfu.ru/portal/docs/F947860695/158_3_est_4.pdf
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author L.G. Shaidarova
A.V. Gedmina
V.D. Demina
I.A. Chelnokova
H.C. Budnikov
author_facet L.G. Shaidarova
A.V. Gedmina
V.D. Demina
I.A. Chelnokova
H.C. Budnikov
author_sort L.G. Shaidarova
collection DOAJ
description Electrodeposited gold and Nafion-gold composite on the surface of glassy carbon electrodes (GCE) have shown electrocatalytic activity during guanine oxidation. In comparison with the unmodified electrode, decreasing of the oxidation potential by 100 mV and increasing of the current of organic compound oxidation have been observed. When the Nafion (NF) film is applied to the surface of the glassy carbon electrode with electrodeposited gold, a five-fold increase of guanine oxidation current has been achieved compared to its oxidation on the modified electrode without the NF film. Conditions have been found for electrodeposition of gold on the surface of the glassy carbon electrode, including that one covered with the NF film, as well as for registration of the maximum catalytic current on these electrodes. Linear dependence of the electrocatalytic response of the modified electrode from the guanine concentration has been observed in the range from 5·10–6 to 5·10–3 mol·L–1 (for Au GCE) and from 5·10–7 to 5·10–3 mol·L–1 (for NF-Au GCE).
format Article
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issn 1815-6169
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language English
publishDate 2016-09-01
publisher Kazan Federal University
record_format Article
series Учёные записки Казанского университета: Серия Естественные науки
spelling doaj-art-0db8957fa9694d0fb18bdd2b2bbd08332025-08-20T03:17:01ZengKazan Federal UniversityУчёные записки Казанского университета: Серия Естественные науки1815-61692500-218X2016-09-011583369380Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion FilmL.G. Shaidarova0A.V. Gedmina1V.D. Demina2I.A. Chelnokova3H.C. Budnikov4Kazan Federal University, Kazan, 420008 RussiaKazan Federal University, Kazan, 420008 RussiaKazan Federal University, Kazan, 420008 RussiaKazan Federal University, Kazan, 420008 RussiaKazan Federal University, Kazan, 420008 RussiaElectrodeposited gold and Nafion-gold composite on the surface of glassy carbon electrodes (GCE) have shown electrocatalytic activity during guanine oxidation. In comparison with the unmodified electrode, decreasing of the oxidation potential by 100 mV and increasing of the current of organic compound oxidation have been observed. When the Nafion (NF) film is applied to the surface of the glassy carbon electrode with electrodeposited gold, a five-fold increase of guanine oxidation current has been achieved compared to its oxidation on the modified electrode without the NF film. Conditions have been found for electrodeposition of gold on the surface of the glassy carbon electrode, including that one covered with the NF film, as well as for registration of the maximum catalytic current on these electrodes. Linear dependence of the electrocatalytic response of the modified electrode from the guanine concentration has been observed in the range from 5·10–6 to 5·10–3 mol·L–1 (for Au GCE) and from 5·10–7 to 5·10–3 mol·L–1 (for NF-Au GCE).http://kpfu.ru/portal/docs/F947860695/158_3_est_4.pdfchemically modified electrodesvoltammetric determination of guanine
spellingShingle L.G. Shaidarova
A.V. Gedmina
V.D. Demina
I.A. Chelnokova
H.C. Budnikov
Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion Film
Учёные записки Казанского университета: Серия Естественные науки
chemically modified electrodes
voltammetric determination of guanine
title Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion Film
title_full Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion Film
title_fullStr Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion Film
title_full_unstemmed Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion Film
title_short Voltammetric Determination of Guanine on the Electrode Modified by Gold Deposit and Nafion Film
title_sort voltammetric determination of guanine on the electrode modified by gold deposit and nafion film
topic chemically modified electrodes
voltammetric determination of guanine
url http://kpfu.ru/portal/docs/F947860695/158_3_est_4.pdf
work_keys_str_mv AT lgshaidarova voltammetricdeterminationofguanineontheelectrodemodifiedbygolddepositandnafionfilm
AT avgedmina voltammetricdeterminationofguanineontheelectrodemodifiedbygolddepositandnafionfilm
AT vddemina voltammetricdeterminationofguanineontheelectrodemodifiedbygolddepositandnafionfilm
AT iachelnokova voltammetricdeterminationofguanineontheelectrodemodifiedbygolddepositandnafionfilm
AT hcbudnikov voltammetricdeterminationofguanineontheelectrodemodifiedbygolddepositandnafionfilm