Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperature

Resolving severe interface reactions and unclear interfacial bonding mechanisms in graphene/Ti matrix composites is imperative for their widespread application in advanced technological domains such as aerospace, defense, and medicine. This study amalgamates density functional theory calculations wi...

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Main Authors: Mengying Yang, Hassaan Ahmad Butt, Yangju Feng, Dmitry Krasnikov, Yucheng Lei, Albert G. Nasibulin, Yaotian Yan, Junlei Qi, Zeyu Wang
Format: Article
Language:English
Published: Elsevier 2025-05-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425007471
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author Mengying Yang
Hassaan Ahmad Butt
Yangju Feng
Dmitry Krasnikov
Yucheng Lei
Albert G. Nasibulin
Yaotian Yan
Junlei Qi
Zeyu Wang
author_facet Mengying Yang
Hassaan Ahmad Butt
Yangju Feng
Dmitry Krasnikov
Yucheng Lei
Albert G. Nasibulin
Yaotian Yan
Junlei Qi
Zeyu Wang
author_sort Mengying Yang
collection DOAJ
description Resolving severe interface reactions and unclear interfacial bonding mechanisms in graphene/Ti matrix composites is imperative for their widespread application in advanced technological domains such as aerospace, defense, and medicine. This study amalgamates density functional theory calculations with experimental investigations to study the interfacial interactive behavior between Ti and graphene with pristine and defective structures. Calculative results reveal the presence of weak interactions between pristine graphene and Ti, which differs from the chemical reaction between defective graphene and Ti. The interfacial bonding characteristics of Ag-Cu-Ti eutectic foils on a pure Cu substrate (P-Cup), Cu substrate with pristine graphene (G-Cup), and Cu substrate with defective graphene (VFG-Cup) were studied through the sessile drop method at a moderate temperature of 880 °C (lower than the melting point of Ti). The Ag-Cu-Ti filler displayed sound wettability on P-Cup, G-Cup, and VFG-Cup. Specifically, the contact angles were approximately 2°, around 6°, and less than 1°, respectively. By observing the interfacial microstructure, pristine graphene is proved to be preserved, indicating that it impedes self-erosion as well as the Cu substrate by the active Ag-Cu-Ti filler. The defect-rich graphene behaves the opposite, aligning with the findings of the density functional theory calculations. This work holds significant potential in guiding the design of graphene-reinforced metal matrix composites.
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spelling doaj-art-0d9cdbf4e0bd4b778c354f7dc1aba4c72025-08-20T03:16:46ZengElsevierJournal of Materials Research and Technology2238-78542025-05-01362064207310.1016/j.jmrt.2025.03.237Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperatureMengying Yang0Hassaan Ahmad Butt1Yangju Feng2Dmitry Krasnikov3Yucheng Lei4Albert G. Nasibulin5Yaotian Yan6Junlei Qi7Zeyu Wang8School of Material Science and Engineering, Jiangsu University, 301 Xuefu Road, Zhenjiang, 212013, ChinaSkolkovo Institute of Science and Technology, Nobel 3, Moscow, 121205, RussiaSchool of Material Science and Engineering, Jiangsu University, 301 Xuefu Road, Zhenjiang, 212013, ChinaSkolkovo Institute of Science and Technology, Nobel 3, Moscow, 121205, RussiaSchool of Material Science and Engineering, Jiangsu University, 301 Xuefu Road, Zhenjiang, 212013, ChinaSkolkovo Institute of Science and Technology, Nobel 3, Moscow, 121205, RussiaState Key Laboratory of Precision Welding & Joining of Materials and Structures, Harbin Institute of Technology, Harbin, 150001, ChinaState Key Laboratory of Precision Welding & Joining of Materials and Structures, Harbin Institute of Technology, Harbin, 150001, ChinaSchool of Material Science and Engineering, Jiangsu University, 301 Xuefu Road, Zhenjiang, 212013, China; Corresponding author.Resolving severe interface reactions and unclear interfacial bonding mechanisms in graphene/Ti matrix composites is imperative for their widespread application in advanced technological domains such as aerospace, defense, and medicine. This study amalgamates density functional theory calculations with experimental investigations to study the interfacial interactive behavior between Ti and graphene with pristine and defective structures. Calculative results reveal the presence of weak interactions between pristine graphene and Ti, which differs from the chemical reaction between defective graphene and Ti. The interfacial bonding characteristics of Ag-Cu-Ti eutectic foils on a pure Cu substrate (P-Cup), Cu substrate with pristine graphene (G-Cup), and Cu substrate with defective graphene (VFG-Cup) were studied through the sessile drop method at a moderate temperature of 880 °C (lower than the melting point of Ti). The Ag-Cu-Ti filler displayed sound wettability on P-Cup, G-Cup, and VFG-Cup. Specifically, the contact angles were approximately 2°, around 6°, and less than 1°, respectively. By observing the interfacial microstructure, pristine graphene is proved to be preserved, indicating that it impedes self-erosion as well as the Cu substrate by the active Ag-Cu-Ti filler. The defect-rich graphene behaves the opposite, aligning with the findings of the density functional theory calculations. This work holds significant potential in guiding the design of graphene-reinforced metal matrix composites.http://www.sciencedirect.com/science/article/pii/S2238785425007471GrapheneTitaniumWetting interfaceDensity functional theory calculations
spellingShingle Mengying Yang
Hassaan Ahmad Butt
Yangju Feng
Dmitry Krasnikov
Yucheng Lei
Albert G. Nasibulin
Yaotian Yan
Junlei Qi
Zeyu Wang
Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperature
Journal of Materials Research and Technology
Graphene
Titanium
Wetting interface
Density functional theory calculations
title Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperature
title_full Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperature
title_fullStr Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperature
title_full_unstemmed Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperature
title_short Revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of Ag-Cu-Ti eutectic alloy at a moderate temperature
title_sort revealing the different metallurgical resistance of pristine and defective graphene to titanium by studying the wetting behavior of ag cu ti eutectic alloy at a moderate temperature
topic Graphene
Titanium
Wetting interface
Density functional theory calculations
url http://www.sciencedirect.com/science/article/pii/S2238785425007471
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