Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal Feed

The main disadvantages of using soybean oil extraction waste as a raw feed material are its high contents of fiber, fat, and anti-nutritional factors. Therefore, several processing methods such as extrusion and hydrolysis are used to overcome these disadvantages and increase the availability of high...

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Main Authors: Marina Belyshkina, Tamara Kobozeva, Mikhail Zagoruiko, Oksana Serebryakova, Maisoon Shaaban, Tatiana Ananeva, Igor Bashmakov
Format: Article
Language:English
Published: MDPI AG 2025-04-01
Series:Fermentation
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Online Access:https://www.mdpi.com/2311-5637/11/4/209
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author Marina Belyshkina
Tamara Kobozeva
Mikhail Zagoruiko
Oksana Serebryakova
Maisoon Shaaban
Tatiana Ananeva
Igor Bashmakov
author_facet Marina Belyshkina
Tamara Kobozeva
Mikhail Zagoruiko
Oksana Serebryakova
Maisoon Shaaban
Tatiana Ananeva
Igor Bashmakov
author_sort Marina Belyshkina
collection DOAJ
description The main disadvantages of using soybean oil extraction waste as a raw feed material are its high contents of fiber, fat, and anti-nutritional factors. Therefore, several processing methods such as extrusion and hydrolysis are used to overcome these disadvantages and increase the availability of high-quality proteins to animals from this by-product. This study is concerned with the hydrolysis of extruded soybean meal in the presence of bacterial alkaline proteases. The effects of various process parameters were investigated to determine the optimal process parameters for hydrolysis in terms of the total free amino acid and amine nitrogen contents. The experiment included two sets of parameters that were selected for comparison: the temperature and pH in ranges of t 45–50 °C, pH 8–11, compared to the temperature and pH ranges of t = 40–45 °C and pH 7–9, using three enzyme/substrate ratios (1:10, 1:20, and 1:30). The protein hydrolysate was stored for three months after it was treated with two different preservatives (sorbic acid and thymol). Based on the results, it was found that the total free amino acid content was higher when the temperature range was 45–50 °C, the pH range was 8–11, and sorbic acid was used as a preservative.
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spelling doaj-art-0d897b8cf0f540ca8e9d78c4a25d97ba2025-08-20T02:28:28ZengMDPI AGFermentation2311-56372025-04-0111420910.3390/fermentation11040209Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal FeedMarina Belyshkina0Tamara Kobozeva1Mikhail Zagoruiko2Oksana Serebryakova3Maisoon Shaaban4Tatiana Ananeva5Igor Bashmakov6Federal State Budgetary Scientific Institution “Federal Scientific Agroengineering Center VIM”, 5. 1st Institutskiy Proezd Str., Moscow 109428, RussiaFederal State Budgetary Scientific Institution “Federal Scientific Agroengineering Center VIM”, 5. 1st Institutskiy Proezd Str., Moscow 109428, RussiaFederal State Budgetary Scientific Institution “Federal Scientific Agroengineering Center VIM”, 5. 1st Institutskiy Proezd Str., Moscow 109428, RussiaFederal State Budgetary Scientific Institution “Federal Scientific Agroengineering Center VIM”, 5. 1st Institutskiy Proezd Str., Moscow 109428, RussiaFederal State Budgetary Scientific Institution “Federal Scientific Agroengineering Center VIM”, 5. 1st Institutskiy Proezd Str., Moscow 109428, RussiaFederal State Budgetary Scientific Institution “Federal Scientific Agroengineering Center VIM”, 5. 1st Institutskiy Proezd Str., Moscow 109428, RussiaFederal State Budgetary Scientific Institution “Federal Scientific Agroengineering Center VIM”, 5. 1st Institutskiy Proezd Str., Moscow 109428, RussiaThe main disadvantages of using soybean oil extraction waste as a raw feed material are its high contents of fiber, fat, and anti-nutritional factors. Therefore, several processing methods such as extrusion and hydrolysis are used to overcome these disadvantages and increase the availability of high-quality proteins to animals from this by-product. This study is concerned with the hydrolysis of extruded soybean meal in the presence of bacterial alkaline proteases. The effects of various process parameters were investigated to determine the optimal process parameters for hydrolysis in terms of the total free amino acid and amine nitrogen contents. The experiment included two sets of parameters that were selected for comparison: the temperature and pH in ranges of t 45–50 °C, pH 8–11, compared to the temperature and pH ranges of t = 40–45 °C and pH 7–9, using three enzyme/substrate ratios (1:10, 1:20, and 1:30). The protein hydrolysate was stored for three months after it was treated with two different preservatives (sorbic acid and thymol). Based on the results, it was found that the total free amino acid content was higher when the temperature range was 45–50 °C, the pH range was 8–11, and sorbic acid was used as a preservative.https://www.mdpi.com/2311-5637/11/4/209amine nitrogenfree amino acidsprotein hydrolysatehydrolysate storagethymolsorbic acid
spellingShingle Marina Belyshkina
Tamara Kobozeva
Mikhail Zagoruiko
Oksana Serebryakova
Maisoon Shaaban
Tatiana Ananeva
Igor Bashmakov
Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal Feed
Fermentation
amine nitrogen
free amino acids
protein hydrolysate
hydrolysate storage
thymol
sorbic acid
title Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal Feed
title_full Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal Feed
title_fullStr Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal Feed
title_full_unstemmed Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal Feed
title_short Determination of the Optimal Biotechnological Parameters for Industrial Production of Protein Hydrolysates for Animal Feed
title_sort determination of the optimal biotechnological parameters for industrial production of protein hydrolysates for animal feed
topic amine nitrogen
free amino acids
protein hydrolysate
hydrolysate storage
thymol
sorbic acid
url https://www.mdpi.com/2311-5637/11/4/209
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AT tamarakobozeva determinationoftheoptimalbiotechnologicalparametersforindustrialproductionofproteinhydrolysatesforanimalfeed
AT mikhailzagoruiko determinationoftheoptimalbiotechnologicalparametersforindustrialproductionofproteinhydrolysatesforanimalfeed
AT oksanaserebryakova determinationoftheoptimalbiotechnologicalparametersforindustrialproductionofproteinhydrolysatesforanimalfeed
AT maisoonshaaban determinationoftheoptimalbiotechnologicalparametersforindustrialproductionofproteinhydrolysatesforanimalfeed
AT tatianaananeva determinationoftheoptimalbiotechnologicalparametersforindustrialproductionofproteinhydrolysatesforanimalfeed
AT igorbashmakov determinationoftheoptimalbiotechnologicalparametersforindustrialproductionofproteinhydrolysatesforanimalfeed