Analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell

The study on the possible use of calcined chicken eggshells as a biosorbent for copper ions removal from aqueous solutions, as well as some comparisons between raw and calcined eggshells, are presented in this paper. SEM- -EDS and FTIR analysis of the calcined chicken eggshell samples were performed...

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Main Authors: Marković Miljan, Gorgievski Milan, Štrbac Nada, Grekulović Vesna, Zdravković Milica, Marković Marina, Stanković Dalibor
Format: Article
Language:English
Published: Serbian Chemical Society 2025-01-01
Series:Journal of the Serbian Chemical Society
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Online Access:https://doiserbia.nb.rs/img/doi/0352-5139/2025/0352-51392500017M.pdf
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author Marković Miljan
Gorgievski Milan
Štrbac Nada
Grekulović Vesna
Zdravković Milica
Marković Marina
Stanković Dalibor
author_facet Marković Miljan
Gorgievski Milan
Štrbac Nada
Grekulović Vesna
Zdravković Milica
Marković Marina
Stanković Dalibor
author_sort Marković Miljan
collection DOAJ
description The study on the possible use of calcined chicken eggshells as a biosorbent for copper ions removal from aqueous solutions, as well as some comparisons between raw and calcined eggshells, are presented in this paper. SEM- -EDS and FTIR analysis of the calcined chicken eggshell samples were performed. In addition, the DTA-TGA analysis on raw chicken eggshells was performed. The influence of various process parameters, such as solution pH, stirring rate, biosorbent mass and Cu2+ concentration, was investigated. The kinetic analysis using four different empirical kinetic models was performed. The equilibrium analysis was done using the Langmuir, Freundlich and Temkin isotherm models. The process was optimized using the response surface methodology based on the Box–Behnken design (RSM-BBD). The obtained results are compared to our previous study on raw eggshells as a biosorbent for Cu2+ removal, in order to determine the justification for biosorbent modification (i.e., the calcination of raw eggshells).
format Article
id doaj-art-0d4c2f2f4c07481daf6a1d5518eab1d0
institution Kabale University
issn 0352-5139
1820-7421
language English
publishDate 2025-01-01
publisher Serbian Chemical Society
record_format Article
series Journal of the Serbian Chemical Society
spelling doaj-art-0d4c2f2f4c07481daf6a1d5518eab1d02025-08-20T03:31:31ZengSerbian Chemical SocietyJournal of the Serbian Chemical Society0352-51391820-74212025-01-0190566168010.2298/JSC241107017M0352-51392500017MAnalysis and statistical modeling of copper ions biosorption onto calcined chicken eggshellMarković Miljan0https://orcid.org/0000-0002-4734-1481Gorgievski Milan1https://orcid.org/0000-0002-9899-719XŠtrbac Nada2https://orcid.org/0000-0003-4836-1350Grekulović Vesna3https://orcid.org/0000-0001-6871-4016Zdravković Milica4https://orcid.org/0000-0001-9488-9151Marković Marina5https://orcid.org/0009-0007-7553-6423Stanković Dalibor6https://orcid.org/0000-0001-7465-1373University of Belgrade, Technical Faculty in Bor, Bor, SerbiaUniversity of Belgrade, Technical Faculty in Bor, Bor, SerbiaUniversity of Belgrade, Technical Faculty in Bor, Bor, SerbiaUniversity of Belgrade, Technical Faculty in Bor, Bor, SerbiaUniversity of Belgrade, Technical Faculty in Bor, Bor, SerbiaUniversity of Belgrade, Technical Faculty in Bor, Bor, SerbiaUniversity of Belgrade, Faculty of Chemistry, Belgrade, SerbiaThe study on the possible use of calcined chicken eggshells as a biosorbent for copper ions removal from aqueous solutions, as well as some comparisons between raw and calcined eggshells, are presented in this paper. SEM- -EDS and FTIR analysis of the calcined chicken eggshell samples were performed. In addition, the DTA-TGA analysis on raw chicken eggshells was performed. The influence of various process parameters, such as solution pH, stirring rate, biosorbent mass and Cu2+ concentration, was investigated. The kinetic analysis using four different empirical kinetic models was performed. The equilibrium analysis was done using the Langmuir, Freundlich and Temkin isotherm models. The process was optimized using the response surface methodology based on the Box–Behnken design (RSM-BBD). The obtained results are compared to our previous study on raw eggshells as a biosorbent for Cu2+ removal, in order to determine the justification for biosorbent modification (i.e., the calcination of raw eggshells).https://doiserbia.nb.rs/img/doi/0352-5139/2025/0352-51392500017M.pdfbiosorptioncalcined chicken eggshellequilibriumkineticsbox-behnken design
spellingShingle Marković Miljan
Gorgievski Milan
Štrbac Nada
Grekulović Vesna
Zdravković Milica
Marković Marina
Stanković Dalibor
Analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell
Journal of the Serbian Chemical Society
biosorption
calcined chicken eggshell
equilibrium
kinetics
box-behnken design
title Analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell
title_full Analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell
title_fullStr Analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell
title_full_unstemmed Analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell
title_short Analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell
title_sort analysis and statistical modeling of copper ions biosorption onto calcined chicken eggshell
topic biosorption
calcined chicken eggshell
equilibrium
kinetics
box-behnken design
url https://doiserbia.nb.rs/img/doi/0352-5139/2025/0352-51392500017M.pdf
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