Micro Determination Study and Organo physical properties Of Resorcinol with Thiamine in the Presence of Potassium Dichromate
Objective: This study aims to estimate Resorcinol (3- hydroxy phenol). Methodology: The study was through the development of a simple and high sensitivity and selectivity to estimate Resorcinol (3- hydroxy phenol) and The method is based on the reaction of Resorcinol (3-hydroxyphenol) with Thiami...
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| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
University of Kufa, Faculty of Nursing
2013-12-01
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| Series: | Kufa Journal for Nursing Sciences |
| Subjects: | |
| Online Access: | https://journal.uokufa.edu.iq/index.php/kjns/article/view/2517 |
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| Summary: | Objective: This study aims to estimate Resorcinol (3- hydroxy phenol).
Methodology: The study was through the development of a simple and high sensitivity and selectivity to estimate Resorcinol (3- hydroxy phenol) and The method is based on the reaction of Resorcinol (3-hydroxyphenol) with Thiamine (Vitamin B1) and potassium Dichromate at pH 3.5. So The reactions gave an intense water soluble color products that have maximum absorption at 510 nm.
Results: This study showed that the ε max for 3- hydroxy phenol is (0.145 Χ 104 liter. Mol-1 .cm-1), A linear correlations (1-9 μg ml-1) for 3-hydroxyphenol compound was found between absorbance at λmax and concentration. The accurate (relative error was better than -0.2 %) and precise ( RSD was better than 1.2%). The colored product was found to be 1:1 (3-hydroxyphenol : Thiamine). The stability constant of the reaction under optimized conditions at room temperature was 3.25 Χ 105 L. mole-1 .
Recommendations: The study recommends the appointment of phenolic compounds or other phenolic derivatives are relying on this method any use of thiamine and oxidized worker himself (potassium dichromate).
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| ISSN: | 2223-4055 2521-8638 |