Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materials

Multi-walled carbon nanotubes/titanium dioxide nanocomposites were successfully synthesized by Sol-Gel method using new different ratios of tetrabutyl titanate and functionalized MWCNTs as the starting precursors. The synthesized Multi-walled carbon nanotubes/different titanium dioxide percentages (...

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Main Authors: Badr A. El-Sayed, Walied A.A. Mohamed, Hoda R. Galal, H.M. Abd El-Bary, Mahmoud A.M. Ahmed
Format: Article
Language:English
Published: Egyptian Petroleum Research Institute 2019-06-01
Series:Egyptian Journal of Petroleum
Online Access:http://www.sciencedirect.com/science/article/pii/S1110062119300947
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author Badr A. El-Sayed
Walied A.A. Mohamed
Hoda R. Galal
H.M. Abd El-Bary
Mahmoud A.M. Ahmed
author_facet Badr A. El-Sayed
Walied A.A. Mohamed
Hoda R. Galal
H.M. Abd El-Bary
Mahmoud A.M. Ahmed
author_sort Badr A. El-Sayed
collection DOAJ
description Multi-walled carbon nanotubes/titanium dioxide nanocomposites were successfully synthesized by Sol-Gel method using new different ratios of tetrabutyl titanate and functionalized MWCNTs as the starting precursors. The synthesized Multi-walled carbon nanotubes/different titanium dioxide percentages (MWCNTs/3, 6 and 10%TiO2) nanocomposites were characterized using XRD, SEM and N2 Adsorption-Desorption techniques. The optical band gap was estimated for MWCNTs and MWCNTs with different TiO2 percentages by Kubelka-Munk equation giving 3.72, 2.92, 2.83, 2.71 eV values respectively. The synthesized nanocomposites were used as photocatalyst for decontamination of two local textile Dianix Blue and Vat Green 1 Dyes which commonly used in dyeing manufacture in local market. Keywords: MWCNTs/x%TiO2 nanocomposites, Sol–gel method, BET, Dianix Blue Dye, Vat Green 1 Dye
format Article
id doaj-art-0a2a834554de4e98ad5f3ebf1ed1b932
institution DOAJ
issn 1110-0621
language English
publishDate 2019-06-01
publisher Egyptian Petroleum Research Institute
record_format Article
series Egyptian Journal of Petroleum
spelling doaj-art-0a2a834554de4e98ad5f3ebf1ed1b9322025-08-20T03:04:43ZengEgyptian Petroleum Research InstituteEgyptian Journal of Petroleum1110-06212019-06-0128224725210.1016/j.ejpe.2019.05.002Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materialsBadr A. El-Sayed0Walied A.A. Mohamed1Hoda R. Galal2H.M. Abd El-Bary3Mahmoud A.M. Ahmed4Department of Chemistry, Faculty of Science, Al-Azhar University, Nasr City, Cairo, Egypt; Corresponding author at: Analytical and Inorganic Chemistry Department, Al Azhar University, Cairo, P.O. 11884, Egypt.Department of Inorganic Chemistry, National Research Centre, Giza, EgyptDepartment of Inorganic Chemistry, National Research Centre, Giza, EgyptDepartment of Chemistry, Faculty of Science, Al-Azhar University, Nasr City, Cairo, EgyptDepartment of Chemistry, Faculty of Science, Al-Azhar University, Nasr City, Cairo, EgyptMulti-walled carbon nanotubes/titanium dioxide nanocomposites were successfully synthesized by Sol-Gel method using new different ratios of tetrabutyl titanate and functionalized MWCNTs as the starting precursors. The synthesized Multi-walled carbon nanotubes/different titanium dioxide percentages (MWCNTs/3, 6 and 10%TiO2) nanocomposites were characterized using XRD, SEM and N2 Adsorption-Desorption techniques. The optical band gap was estimated for MWCNTs and MWCNTs with different TiO2 percentages by Kubelka-Munk equation giving 3.72, 2.92, 2.83, 2.71 eV values respectively. The synthesized nanocomposites were used as photocatalyst for decontamination of two local textile Dianix Blue and Vat Green 1 Dyes which commonly used in dyeing manufacture in local market. Keywords: MWCNTs/x%TiO2 nanocomposites, Sol–gel method, BET, Dianix Blue Dye, Vat Green 1 Dyehttp://www.sciencedirect.com/science/article/pii/S1110062119300947
spellingShingle Badr A. El-Sayed
Walied A.A. Mohamed
Hoda R. Galal
H.M. Abd El-Bary
Mahmoud A.M. Ahmed
Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materials
Egyptian Journal of Petroleum
title Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materials
title_full Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materials
title_fullStr Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materials
title_full_unstemmed Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materials
title_short Photocatalytic study of some synthesized MWCNTs/TiO2 nanocomposites used in the treatment of industrial hazard materials
title_sort photocatalytic study of some synthesized mwcnts tio2 nanocomposites used in the treatment of industrial hazard materials
url http://www.sciencedirect.com/science/article/pii/S1110062119300947
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AT waliedaamohamed photocatalyticstudyofsomesynthesizedmwcntstio2nanocompositesusedinthetreatmentofindustrialhazardmaterials
AT hodargalal photocatalyticstudyofsomesynthesizedmwcntstio2nanocompositesusedinthetreatmentofindustrialhazardmaterials
AT hmabdelbary photocatalyticstudyofsomesynthesizedmwcntstio2nanocompositesusedinthetreatmentofindustrialhazardmaterials
AT mahmoudamahmed photocatalyticstudyofsomesynthesizedmwcntstio2nanocompositesusedinthetreatmentofindustrialhazardmaterials