Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid
The chemical preparation and crystal structure of styphnic acid and naphthalene-1,4-diol (1 : 1) (I) have been reported. The compound crystallizes in the orthorhombic system in space group Pnma and cell parameters a=6.6712(2), b=16.8267(7), c=13.6450(5) Å and V=1531.71(10) Å3, and Z=4. Crystal struc...
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| Format: | Article |
| Language: | English |
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Wiley
2013-01-01
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| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2013/107515 |
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| author | Moamen S. Refat Hossam A. Saad Mohamed Y. El-Sayed Abdel Majid A. Adam Okan Zafer Yeşilel Murat Taş |
| author_facet | Moamen S. Refat Hossam A. Saad Mohamed Y. El-Sayed Abdel Majid A. Adam Okan Zafer Yeşilel Murat Taş |
| author_sort | Moamen S. Refat |
| collection | DOAJ |
| description | The chemical preparation and crystal structure of styphnic acid and naphthalene-1,4-diol (1 : 1) (I) have been reported. The compound crystallizes in the orthorhombic system in space group Pnma and cell parameters a=6.6712(2), b=16.8267(7), c=13.6450(5) Å and V=1531.71(10) Å3, and Z=4. Crystal structure has been determined and refined to R=0.0576. The crystal structure of I, the asymmetric unit, contains C6H2N3O7, C10H7O, and it is a half portion of both styphnic acid and naphthalene-1,4-diol. The O1–H1⋯O2 intramolecular hydrogen bond was found between the O–H and a nitro group in the styphnic acid unit. |
| format | Article |
| id | doaj-art-098b3d01b77f4aea996bcd8778c0ff2f |
| institution | Kabale University |
| issn | 2090-9063 2090-9071 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Chemistry |
| spelling | doaj-art-098b3d01b77f4aea996bcd8778c0ff2f2025-02-03T01:24:27ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/107515107515Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic AcidMoamen S. Refat0Hossam A. Saad1Mohamed Y. El-Sayed2Abdel Majid A. Adam3Okan Zafer Yeşilel4Murat Taş5Chemistry Department, Faculty of Science, Taif University, Al-Haweiah, P.O. Box 888, Taif 21974, Saudi ArabiaChemistry Department, Faculty of Science, Taif University, Al-Haweiah, P.O. Box 888, Taif 21974, Saudi ArabiaChemistry Department, Faculty of Science, Zagazig University, Zagazig, EgyptChemistry Department, Faculty of Science, Taif University, Al-Haweiah, P.O. Box 888, Taif 21974, Saudi ArabiaOsman Gazi University, Art and Science Faculty, Department of Chemistry, Eskişehir, TurkeyGiresun University, Art and Science Faculty, Department of Chemistry, Giresun, TurkeyThe chemical preparation and crystal structure of styphnic acid and naphthalene-1,4-diol (1 : 1) (I) have been reported. The compound crystallizes in the orthorhombic system in space group Pnma and cell parameters a=6.6712(2), b=16.8267(7), c=13.6450(5) Å and V=1531.71(10) Å3, and Z=4. Crystal structure has been determined and refined to R=0.0576. The crystal structure of I, the asymmetric unit, contains C6H2N3O7, C10H7O, and it is a half portion of both styphnic acid and naphthalene-1,4-diol. The O1–H1⋯O2 intramolecular hydrogen bond was found between the O–H and a nitro group in the styphnic acid unit.http://dx.doi.org/10.1155/2013/107515 |
| spellingShingle | Moamen S. Refat Hossam A. Saad Mohamed Y. El-Sayed Abdel Majid A. Adam Okan Zafer Yeşilel Murat Taş Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid Journal of Chemistry |
| title | Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid |
| title_full | Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid |
| title_fullStr | Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid |
| title_full_unstemmed | Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid |
| title_short | Supramolecular Arrangement in Styphnic Acid and Naphthalene-1,4-diol (1 : 1) through a Novel Synthetic Rote for Styphnic Acid |
| title_sort | supramolecular arrangement in styphnic acid and naphthalene 1 4 diol 1 1 through a novel synthetic rote for styphnic acid |
| url | http://dx.doi.org/10.1155/2013/107515 |
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