Layer-by-Layer Assembly and Photocatalytic Activity of Titania Nanosheets on Coal Fly Ash Microspheres

In order to address the problem with titania distribution and recovery, series of Ti0.91O2/CFA photocatalysts (Ti0.91O2/CFA-n, n=2,4,6, and 8) were fabricated by assembling Ti0.91O2 nanosheets on coal fly ash (CFA) microspheres via the layer-by-layer assembly (LBLA) process and characterized by scan...

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Bibliographic Details
Main Authors: Xing Cui, Jianwen Shi, Zhilong Ye, Zhaoji Zhang, Bin Xu, Shaohua Chen
Format: Article
Language:English
Published: Wiley 2014-01-01
Series:International Journal of Photoenergy
Online Access:http://dx.doi.org/10.1155/2014/823078
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Summary:In order to address the problem with titania distribution and recovery, series of Ti0.91O2/CFA photocatalysts (Ti0.91O2/CFA-n, n=2,4,6, and 8) were fabricated by assembling Ti0.91O2 nanosheets on coal fly ash (CFA) microspheres via the layer-by-layer assembly (LBLA) process and characterized by scanning electron microscopy (SEM), X-ray diffraction analysis (XRD), N2-sorption, and ultraviolet-visible absorption (UV-vis) techniques. The SEM images and UV-vis spectra illustrated that Ti0.91O2 nanosheets were immobilized successfully on the CFA by the LBLA approach and changed the characteristics of CFA noticeably. The photocatalytic activity of Ti0.91O2/CFA was evaluated by the photodegradation of methylene blue (MB) under UV irradiation. The results demonstrated that Ti0.91O2/CFA-6 showed the best photocatalytic activity among the series of Ti0.91O2/CFA irradiated for 60 min, with a decoloration rate above 43%. After photocatalysis, the Ti0.91O2/CFA could be easily separated and recycled from aqueous solution and Ti0.91O2 nanosheets were still anchored on the CFA.
ISSN:1110-662X
1687-529X