Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factors

Elastomeric materials, such as silicone rubber, are widely used in engineering applications due to their high deformability and viscoelastic properties. Under quasistatic regime and small deformations their behavior can be considered purely elastic and can be characterized by the elastic modulus, sh...

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Main Authors: Julen Cortazar-Noguerol, Fernando Cortés, Iker Agirre-Olabide, María Jesús Elejabarrieta
Format: Article
Language:English
Published: Elsevier 2025-08-01
Series:Polymer Testing
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Online Access:http://www.sciencedirect.com/science/article/pii/S0142941825001722
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author Julen Cortazar-Noguerol
Fernando Cortés
Iker Agirre-Olabide
María Jesús Elejabarrieta
author_facet Julen Cortazar-Noguerol
Fernando Cortés
Iker Agirre-Olabide
María Jesús Elejabarrieta
author_sort Julen Cortazar-Noguerol
collection DOAJ
description Elastomeric materials, such as silicone rubber, are widely used in engineering applications due to their high deformability and viscoelastic properties. Under quasistatic regime and small deformations their behavior can be considered purely elastic and can be characterized by the elastic modulus, shear modulus, and Poisson's ratio, which are interrelated in isotropic materials. Although standard methodologies exist for determining these properties, experimental measurements are known to be affected by the geometry of the tested samples. The influence of sample geometry on compressive modulus measurements is well understood, however, its effect on shear modulus measurements is less explored. This study investigates how the dimensions of cylindrical samples influence the experimental determination of both the compressive and shear moduli and, consequently, Poisson's ratio. Compression and torsion tests are performed on silicone rubber samples of varying diameters and lengths using a dynamic mechanical analyzer and a rheometer respectively. The results confirm that both the compressive and shear moduli are affected by sample geometry, leading to unrealistic values of Poisson's ratio. To account for these effects, a correction model is proposed for shear modulus measurements, complementing existing corrections for compressive tests. The model successfully describes experimental trends and provides a more reliable estimation of Poisson's ratio, aligning with theoretical expectations for nearly incompressible elastomers. These findings emphasize the importance of considering geometric effects in compressive and torsion tests and provide a framework for improving the accuracy of mechanical characterization in elastomeric materials.
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spelling doaj-art-0790f4aec61d430ca3fc2c71c8d25dc32025-08-20T02:33:19ZengElsevierPolymer Testing1873-23482025-08-0114910885810.1016/j.polymertesting.2025.108858Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factorsJulen Cortazar-Noguerol0Fernando Cortés1Iker Agirre-Olabide2María Jesús Elejabarrieta3Department of Mechanics, Design and Industrial Management, University of Deusto, Avda. de las Universidades 24, 48007, Bilbao, Spain; Corresponding author.Department of Mechanics, Design and Industrial Management, University of Deusto, Avda. de las Universidades 24, 48007, Bilbao, SpainEngineering Department, Public University of Navarre (UPNA), Arrosadia Campus, 31006, Pamplona, SpainDepartment of Mechanics, Design and Industrial Management, University of Deusto, Avda. de las Universidades 24, 48007, Bilbao, SpainElastomeric materials, such as silicone rubber, are widely used in engineering applications due to their high deformability and viscoelastic properties. Under quasistatic regime and small deformations their behavior can be considered purely elastic and can be characterized by the elastic modulus, shear modulus, and Poisson's ratio, which are interrelated in isotropic materials. Although standard methodologies exist for determining these properties, experimental measurements are known to be affected by the geometry of the tested samples. The influence of sample geometry on compressive modulus measurements is well understood, however, its effect on shear modulus measurements is less explored. This study investigates how the dimensions of cylindrical samples influence the experimental determination of both the compressive and shear moduli and, consequently, Poisson's ratio. Compression and torsion tests are performed on silicone rubber samples of varying diameters and lengths using a dynamic mechanical analyzer and a rheometer respectively. The results confirm that both the compressive and shear moduli are affected by sample geometry, leading to unrealistic values of Poisson's ratio. To account for these effects, a correction model is proposed for shear modulus measurements, complementing existing corrections for compressive tests. The model successfully describes experimental trends and provides a more reliable estimation of Poisson's ratio, aligning with theoretical expectations for nearly incompressible elastomers. These findings emphasize the importance of considering geometric effects in compressive and torsion tests and provide a framework for improving the accuracy of mechanical characterization in elastomeric materials.http://www.sciencedirect.com/science/article/pii/S0142941825001722Compression testsTorsional rheometryShape factor effectsCorrection modelsPoisson's ratioElastomeric materials
spellingShingle Julen Cortazar-Noguerol
Fernando Cortés
Iker Agirre-Olabide
María Jesús Elejabarrieta
Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factors
Polymer Testing
Compression tests
Torsional rheometry
Shape factor effects
Correction models
Poisson's ratio
Elastomeric materials
title Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factors
title_full Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factors
title_fullStr Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factors
title_full_unstemmed Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factors
title_short Compression and torsion testing for elastic moduli and Poisson's ratio characterization in silicone rubber samples with varying shape factors
title_sort compression and torsion testing for elastic moduli and poisson s ratio characterization in silicone rubber samples with varying shape factors
topic Compression tests
Torsional rheometry
Shape factor effects
Correction models
Poisson's ratio
Elastomeric materials
url http://www.sciencedirect.com/science/article/pii/S0142941825001722
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