Synthesis of New Some Imidazole Derivatives Containing ?-Lactam Ring

In this work 5-methylene-yl - (2-methy –oxazole-4-one) (1H) imidazole (1) were synthesized from the reaction of L-Histidine with acetic anhydride and which converted to the of 5-methylene-yl-(2-methyl 3-amino imidazole-4-one)-1H-imidazole (2) by reaction with hydrazine hydrate. Schiff bases (3-6) we...

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Main Author: Baghdad Science Journal
Format: Article
Language:English
Published: University of Baghdad, College of Science for Women 2016-06-01
Series:مجلة بغداد للعلوم
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Online Access:http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2776
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author Baghdad Science Journal
author_facet Baghdad Science Journal
author_sort Baghdad Science Journal
collection DOAJ
description In this work 5-methylene-yl - (2-methy –oxazole-4-one) (1H) imidazole (1) were synthesized from the reaction of L-Histidine with acetic anhydride and which converted to the of 5-methylene-yl-(2-methyl 3-amino imidazole-4-one)-1H-imidazole (2) by reaction with hydrazine hydrate. Schiff bases (3-6) were synthesized from the reaction of compound (2) with different aromatic aldehyde. Reaction of compounds (3-6) with chloroacetyl chloride gives azetidinone one derivatives (7-10). These compounds were characterized by FT-IR and some of them with 1H-NMR and 13C-NMR spectroscopy.
format Article
id doaj-art-05f7da7dc2c645479286ebc331f2ad9e
institution Kabale University
issn 2078-8665
2411-7986
language English
publishDate 2016-06-01
publisher University of Baghdad, College of Science for Women
record_format Article
series مجلة بغداد للعلوم
spelling doaj-art-05f7da7dc2c645479286ebc331f2ad9e2025-08-20T03:34:20ZengUniversity of Baghdad, College of Science for Womenمجلة بغداد للعلوم2078-86652411-79862016-06-0113210.21123/bsj.13.2.307-316Synthesis of New Some Imidazole Derivatives Containing ?-Lactam RingBaghdad Science JournalIn this work 5-methylene-yl - (2-methy –oxazole-4-one) (1H) imidazole (1) were synthesized from the reaction of L-Histidine with acetic anhydride and which converted to the of 5-methylene-yl-(2-methyl 3-amino imidazole-4-one)-1H-imidazole (2) by reaction with hydrazine hydrate. Schiff bases (3-6) were synthesized from the reaction of compound (2) with different aromatic aldehyde. Reaction of compounds (3-6) with chloroacetyl chloride gives azetidinone one derivatives (7-10). These compounds were characterized by FT-IR and some of them with 1H-NMR and 13C-NMR spectroscopy.http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2776"L-Histidine, Schiff base, Imidzole."
spellingShingle Baghdad Science Journal
Synthesis of New Some Imidazole Derivatives Containing ?-Lactam Ring
مجلة بغداد للعلوم
"L-Histidine, Schiff base, Imidzole."
title Synthesis of New Some Imidazole Derivatives Containing ?-Lactam Ring
title_full Synthesis of New Some Imidazole Derivatives Containing ?-Lactam Ring
title_fullStr Synthesis of New Some Imidazole Derivatives Containing ?-Lactam Ring
title_full_unstemmed Synthesis of New Some Imidazole Derivatives Containing ?-Lactam Ring
title_short Synthesis of New Some Imidazole Derivatives Containing ?-Lactam Ring
title_sort synthesis of new some imidazole derivatives containing lactam ring
topic "L-Histidine, Schiff base, Imidzole."
url http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2776
work_keys_str_mv AT baghdadsciencejournal synthesisofnewsomeimidazolederivativescontaininglactamring