Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEO

In order to improve the catalytic property of Fe-based Fenton catalysts, a sulfur-modified Fe3O4&#x00A0;coating Fenton-like catalyst was successfully prepared on titanium alloy via plasma electrolytic oxidation. The effect of the concentration of iron source K3[Fe(CN)6] in the electrolyte on the...

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Main Author: ZHOU Yang, ZHANG Xiao, XIA Qi-xing, CHEN Chang-ju, YAO Zhong-ping
Format: Article
Language:zho
Published: Editorial Department of Materials Protection 2021-08-01
Series:Cailiao Baohu
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Online Access:http://www.mat-pro.com/fileup/1001-1560/PDF/20210801.pdf
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author ZHOU Yang, ZHANG Xiao, XIA Qi-xing, CHEN Chang-ju, YAO Zhong-ping
author_facet ZHOU Yang, ZHANG Xiao, XIA Qi-xing, CHEN Chang-ju, YAO Zhong-ping
author_sort ZHOU Yang, ZHANG Xiao, XIA Qi-xing, CHEN Chang-ju, YAO Zhong-ping
collection DOAJ
description In order to improve the catalytic property of Fe-based Fenton catalysts, a sulfur-modified Fe3O4&#x00A0;coating Fenton-like catalyst was successfully prepared on titanium alloy via plasma electrolytic oxidation. The effect of the concentration of iron source K3[Fe(CN)6] in the electrolyte on the structural composition and phenol degradation performance of the coating was studied. In addition, the surface morphology and phase composition of the catalyst were characterized by SEM, EDS and XRD, and phenol was used as the target degradation product to evaluate the Fenton-like catalytic activity. Results showed that when the concentration of K3[Fe(CN)6] in the electrolyte increased, the Fe3O4&#x00A0;composition in the film increased, the sulfur-containing groups decreased, and the pore size and number of pores on the surface of the coating also changed. Phenol degradation experiments displayed that the sulfur-modified Fe3O4&#x00A0;coating had good catalytic activity under near-neutral conditions.
format Article
id doaj-art-0581dabf650b409ea3b535b4ba4297c9
institution Kabale University
issn 1001-1560
language zho
publishDate 2021-08-01
publisher Editorial Department of Materials Protection
record_format Article
series Cailiao Baohu
spelling doaj-art-0581dabf650b409ea3b535b4ba4297c92025-08-20T03:28:47ZzhoEditorial Department of Materials ProtectionCailiao Baohu1001-15602021-08-01548110.16577/j.cnki.42-1215/tb.2021.08.001Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEOZHOU Yang, ZHANG Xiao, XIA Qi-xing, CHEN Chang-ju, YAO Zhong-ping0School of Chemistry and Chemical Engineering, Harbin Institute of Technology, Harbin 150001, ChinaIn order to improve the catalytic property of Fe-based Fenton catalysts, a sulfur-modified Fe3O4&#x00A0;coating Fenton-like catalyst was successfully prepared on titanium alloy via plasma electrolytic oxidation. The effect of the concentration of iron source K3[Fe(CN)6] in the electrolyte on the structural composition and phenol degradation performance of the coating was studied. In addition, the surface morphology and phase composition of the catalyst were characterized by SEM, EDS and XRD, and phenol was used as the target degradation product to evaluate the Fenton-like catalytic activity. Results showed that when the concentration of K3[Fe(CN)6] in the electrolyte increased, the Fe3O4&#x00A0;composition in the film increased, the sulfur-containing groups decreased, and the pore size and number of pores on the surface of the coating also changed. Phenol degradation experiments displayed that the sulfur-modified Fe3O4&#x00A0;coating had good catalytic activity under near-neutral conditions.http://www.mat-pro.com/fileup/1001-1560/PDF/20210801.pdfplasma electrolytic oxidation; fenton-like catalyst; iron oxide coatings; structure; degradation performance; phenol
spellingShingle ZHOU Yang, ZHANG Xiao, XIA Qi-xing, CHEN Chang-ju, YAO Zhong-ping
Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEO
Cailiao Baohu
plasma electrolytic oxidation; fenton-like catalyst; iron oxide coatings; structure; degradation performance; phenol
title Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEO
title_full Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEO
title_fullStr Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEO
title_full_unstemmed Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEO
title_short Effect of K<sub>3</sub>[Fe(CN)<sub>6</sub>] Concentration on the Structure and DegradationPerformance of Sulfur - Modified Fe<sub>3</sub>O<sub>4</sub> Coating Prepared by PEO
title_sort effect of k sub 3 sub fe cn sub 6 sub concentration on the structure and degradationperformance of sulfur modified fe sub 3 sub o sub 4 sub coating prepared by peo
topic plasma electrolytic oxidation; fenton-like catalyst; iron oxide coatings; structure; degradation performance; phenol
url http://www.mat-pro.com/fileup/1001-1560/PDF/20210801.pdf
work_keys_str_mv AT zhouyangzhangxiaoxiaqixingchenchangjuyaozhongping effectofksub3subfecnsub6subconcentrationonthestructureanddegradationperformanceofsulfurmodifiedfesub3subosub4subcoatingpreparedbypeo