Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortus

The acetylcholine-gated chloride channel (ACC) family in parasitic nematodes represents a promising target for anthelmintic drug development. Levamisole, a widely known and utilized cholinergic agonist, has been used for decades to address many types of parasitic infections by targeting nematode nic...

Full description

Saved in:
Bibliographic Details
Main Authors: Autumn Collins, Sierra Varley, Tobias Clark, Nathan Chubb, Sean Forrester, Jean-Paul Desaulniers
Format: Article
Language:English
Published: Elsevier 2025-04-01
Series:International Journal for Parasitology: Drugs and Drug Resistance
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2211320725000107
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850203357607624704
author Autumn Collins
Sierra Varley
Tobias Clark
Nathan Chubb
Sean Forrester
Jean-Paul Desaulniers
author_facet Autumn Collins
Sierra Varley
Tobias Clark
Nathan Chubb
Sean Forrester
Jean-Paul Desaulniers
author_sort Autumn Collins
collection DOAJ
description The acetylcholine-gated chloride channel (ACC) family in parasitic nematodes represents a promising target for anthelmintic drug development. Levamisole, a widely known and utilized cholinergic agonist, has been used for decades to address many types of parasitic infections by targeting nematode nicotinic acetylcholine receptors (nAChRs) in nematodes. In this study, we report the synthesis and pharmacological evaluation of eight levamisole derivatives, five of which are novel, on the H. contortus ACC-2 receptor. This includes a CF3-derivatized compound we have identified as compound 6 whose structure contains levamisole as a backbone with the addition of a 2-trifluoromethyl benzyl group. Electrophysiological assays revealed that compound 6 exhibited a five-fold increase in sensitivity (EC50 20 μM) compared to levamisole (EC50 100 μM), our parent compound, with an EC50 comparable to that of acetylcholine (20 μM). Investigation of the in silico docking of compound 6 with H. contortus ACC-2 suggest that it interacts uniquely within the H. contortus ACC-2 binding pocket, which may contribute to its increased receptor sensitivity. These findings highlight the potential of structural modifications containing an electron-withdrawing group at the 2-position which can significantly enhance activity at the H. contortus ACC-2 receptor. This opens many avenues for the development of more effective treatments against parasitic nematodes, in an environment with increasing resistance.
format Article
id doaj-art-03b88a4f387445bc8aff558f229d9bb6
institution OA Journals
issn 2211-3207
language English
publishDate 2025-04-01
publisher Elsevier
record_format Article
series International Journal for Parasitology: Drugs and Drug Resistance
spelling doaj-art-03b88a4f387445bc8aff558f229d9bb62025-08-20T02:11:33ZengElsevierInternational Journal for Parasitology: Drugs and Drug Resistance2211-32072025-04-012710058710.1016/j.ijpddr.2025.100587Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortusAutumn Collins0Sierra Varley1Tobias Clark2Nathan Chubb3Sean Forrester4Jean-Paul Desaulniers5Applied Bioscience Graduate Program, Faculty of Science, University of Ontario Institute of Technology, 2000 Simcoe Street North, Oshawa, ON, L1G 0C5, CanadaApplied Bioscience Graduate Program, Faculty of Science, University of Ontario Institute of Technology, 2000 Simcoe Street North, Oshawa, ON, L1G 0C5, CanadaZoetis, Veterinary Medicine Research and Development, 300 Portage Street, Kalamazoo, MI, 49007, USAZoetis, Veterinary Medicine Research and Development, 300 Portage Street, Kalamazoo, MI, 49007, USAApplied Bioscience Graduate Program, Faculty of Science, University of Ontario Institute of Technology, 2000 Simcoe Street North, Oshawa, ON, L1G 0C5, Canada; Corresponding author.Applied Bioscience Graduate Program, Faculty of Science, University of Ontario Institute of Technology, 2000 Simcoe Street North, Oshawa, ON, L1G 0C5, Canada; Corresponding author.The acetylcholine-gated chloride channel (ACC) family in parasitic nematodes represents a promising target for anthelmintic drug development. Levamisole, a widely known and utilized cholinergic agonist, has been used for decades to address many types of parasitic infections by targeting nematode nicotinic acetylcholine receptors (nAChRs) in nematodes. In this study, we report the synthesis and pharmacological evaluation of eight levamisole derivatives, five of which are novel, on the H. contortus ACC-2 receptor. This includes a CF3-derivatized compound we have identified as compound 6 whose structure contains levamisole as a backbone with the addition of a 2-trifluoromethyl benzyl group. Electrophysiological assays revealed that compound 6 exhibited a five-fold increase in sensitivity (EC50 20 μM) compared to levamisole (EC50 100 μM), our parent compound, with an EC50 comparable to that of acetylcholine (20 μM). Investigation of the in silico docking of compound 6 with H. contortus ACC-2 suggest that it interacts uniquely within the H. contortus ACC-2 binding pocket, which may contribute to its increased receptor sensitivity. These findings highlight the potential of structural modifications containing an electron-withdrawing group at the 2-position which can significantly enhance activity at the H. contortus ACC-2 receptor. This opens many avenues for the development of more effective treatments against parasitic nematodes, in an environment with increasing resistance.http://www.sciencedirect.com/science/article/pii/S2211320725000107Haemonchus contortusAnthelminticAcetylcholine-gated chloride channelLevamisoleDrug discovery
spellingShingle Autumn Collins
Sierra Varley
Tobias Clark
Nathan Chubb
Sean Forrester
Jean-Paul Desaulniers
Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortus
International Journal for Parasitology: Drugs and Drug Resistance
Haemonchus contortus
Anthelmintic
Acetylcholine-gated chloride channel
Levamisole
Drug discovery
title Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortus
title_full Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortus
title_fullStr Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortus
title_full_unstemmed Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortus
title_short Increased activity of CF3-derivatized levamisole at the ACC-2 receptor from the parasitic nematode Haemonchus contortus
title_sort increased activity of cf3 derivatized levamisole at the acc 2 receptor from the parasitic nematode haemonchus contortus
topic Haemonchus contortus
Anthelmintic
Acetylcholine-gated chloride channel
Levamisole
Drug discovery
url http://www.sciencedirect.com/science/article/pii/S2211320725000107
work_keys_str_mv AT autumncollins increasedactivityofcf3derivatizedlevamisoleattheacc2receptorfromtheparasiticnematodehaemonchuscontortus
AT sierravarley increasedactivityofcf3derivatizedlevamisoleattheacc2receptorfromtheparasiticnematodehaemonchuscontortus
AT tobiasclark increasedactivityofcf3derivatizedlevamisoleattheacc2receptorfromtheparasiticnematodehaemonchuscontortus
AT nathanchubb increasedactivityofcf3derivatizedlevamisoleattheacc2receptorfromtheparasiticnematodehaemonchuscontortus
AT seanforrester increasedactivityofcf3derivatizedlevamisoleattheacc2receptorfromtheparasiticnematodehaemonchuscontortus
AT jeanpauldesaulniers increasedactivityofcf3derivatizedlevamisoleattheacc2receptorfromtheparasiticnematodehaemonchuscontortus