Purification of Flake Graphite in a Certain Area of Madagascar

This is an article in the field of mineral processing engineering. The flake graphite flotation concentrate in Madagascar was purified by hydrofluoric acid method. The grade of raw material flake graphite was 94.96%. Based on the single-factor condition tests, the purification process was establishe...

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Main Authors: Zhenmin ZHAI, Yangshuai QIU, Lingyan ZHANG, Zhenfei MAO, Shaochuan DU, Yu ZHANG
Format: Article
Language:zho
Published: Institute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological Sciences 2024-12-01
Series:Kuangchan zonghe liyong
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Online Access:http://www.kczhly.com/en/article/doi/10.3969/j.issn.1000-6532.2024.06.021
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author Zhenmin ZHAI
Yangshuai QIU
Lingyan ZHANG
Zhenfei MAO
Shaochuan DU
Yu ZHANG
author_facet Zhenmin ZHAI
Yangshuai QIU
Lingyan ZHANG
Zhenfei MAO
Shaochuan DU
Yu ZHANG
author_sort Zhenmin ZHAI
collection DOAJ
description This is an article in the field of mineral processing engineering. The flake graphite flotation concentrate in Madagascar was purified by hydrofluoric acid method. The grade of raw material flake graphite was 94.96%. Based on the single-factor condition tests, the purification process was established that the mixture of hydrochloric acid and hydrofluoric acid was 3.5 mL/g, HF volume fraction was 40%, and the graphite grade could be purified to 99.98% by water bath reaction at 60 ℃ for 8 h. In view of the poor purification effect of fine graphite, the graphite was screened and classification before purification. The fine graphite class was subjected to ultrasonic shock pretreatment test, and acid leaching was carried out for purification after 60 min of ultrasonic shock. After purification, the fixed carbon content of fine graphite class was ≥99.92%.
format Article
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institution Kabale University
issn 1000-6532
language zho
publishDate 2024-12-01
publisher Institute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological Sciences
record_format Article
series Kuangchan zonghe liyong
spelling doaj-art-02b567e9b82b4a888b6fd961d8b756072025-01-16T07:32:24ZzhoInstitute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological SciencesKuangchan zonghe liyong1000-65322024-12-0145613514010.3969/j.issn.1000-6532.2024.06.0212025-01zhaizhenminPurification of Flake Graphite in a Certain Area of MadagascarZhenmin ZHAI0Yangshuai QIU1Lingyan ZHANG2Zhenfei MAO3Shaochuan DU4Yu ZHANG5School of Resources and Environmental Engineering, Wuhan University of Technology, Wuhan 430070, Hubei, ChinaSchool of Resources and Environmental Engineering, Wuhan University of Technology, Wuhan 430070, Hubei, ChinaSchool of Resources and Environmental Engineering, Wuhan University of Technology, Wuhan 430070, Hubei, ChinaSchool of Resources and Environmental Engineering, Wuhan University of Technology, Wuhan 430070, Hubei, ChinaSchool of Resources and Environmental Engineering, Wuhan University of Technology, Wuhan 430070, Hubei, ChinaSchool of Resources and Environmental Engineering, Wuhan University of Technology, Wuhan 430070, Hubei, ChinaThis is an article in the field of mineral processing engineering. The flake graphite flotation concentrate in Madagascar was purified by hydrofluoric acid method. The grade of raw material flake graphite was 94.96%. Based on the single-factor condition tests, the purification process was established that the mixture of hydrochloric acid and hydrofluoric acid was 3.5 mL/g, HF volume fraction was 40%, and the graphite grade could be purified to 99.98% by water bath reaction at 60 ℃ for 8 h. In view of the poor purification effect of fine graphite, the graphite was screened and classification before purification. The fine graphite class was subjected to ultrasonic shock pretreatment test, and acid leaching was carried out for purification after 60 min of ultrasonic shock. After purification, the fixed carbon content of fine graphite class was ≥99.92%.http://www.kczhly.com/en/article/doi/10.3969/j.issn.1000-6532.2024.06.021mineral processing engineeringgraphite purificationhydrofluoric acid methodscreening classificationultrasonic shock pretreatment
spellingShingle Zhenmin ZHAI
Yangshuai QIU
Lingyan ZHANG
Zhenfei MAO
Shaochuan DU
Yu ZHANG
Purification of Flake Graphite in a Certain Area of Madagascar
Kuangchan zonghe liyong
mineral processing engineering
graphite purification
hydrofluoric acid method
screening classification
ultrasonic shock pretreatment
title Purification of Flake Graphite in a Certain Area of Madagascar
title_full Purification of Flake Graphite in a Certain Area of Madagascar
title_fullStr Purification of Flake Graphite in a Certain Area of Madagascar
title_full_unstemmed Purification of Flake Graphite in a Certain Area of Madagascar
title_short Purification of Flake Graphite in a Certain Area of Madagascar
title_sort purification of flake graphite in a certain area of madagascar
topic mineral processing engineering
graphite purification
hydrofluoric acid method
screening classification
ultrasonic shock pretreatment
url http://www.kczhly.com/en/article/doi/10.3969/j.issn.1000-6532.2024.06.021
work_keys_str_mv AT zhenminzhai purificationofflakegraphiteinacertainareaofmadagascar
AT yangshuaiqiu purificationofflakegraphiteinacertainareaofmadagascar
AT lingyanzhang purificationofflakegraphiteinacertainareaofmadagascar
AT zhenfeimao purificationofflakegraphiteinacertainareaofmadagascar
AT shaochuandu purificationofflakegraphiteinacertainareaofmadagascar
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