Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interface

The microstructure on the solid-state diffusion bonding interfaces of the initially as-forged, as-solution, and sub-aging FGH96 was characterized, the tensile properties of the bonding interfaces were tested, and the failure behavior was studied. It is found that the good metallurgical bonding is ac...

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Main Authors: YANG Jie, LIU Guang-xu, ZHANG Jing, WANG Wen-ying, WANG Xiao-feng, ZOU Jin-wen
Format: Article
Language:zho
Published: Editorial Office of Powder Metallurgy Technology 2021-08-01
Series:Fenmo yejin jishu
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Online Access:https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2021040005
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author YANG Jie
LIU Guang-xu
ZHANG Jing
WANG Wen-ying
WANG Xiao-feng
ZOU Jin-wen
author_facet YANG Jie
LIU Guang-xu
ZHANG Jing
WANG Wen-ying
WANG Xiao-feng
ZOU Jin-wen
author_sort YANG Jie
collection DOAJ
description The microstructure on the solid-state diffusion bonding interfaces of the initially as-forged, as-solution, and sub-aging FGH96 was characterized, the tensile properties of the bonding interfaces were tested, and the failure behavior was studied. It is found that the good metallurgical bonding is achieved at the bonding interfaces of all the three primitive state specimens after the solid-state diffusion, and no cracks and cavities are found. The interfaces of the as-forged specimens show more sufficient diffusion of elements and smoother transition of microstructure, while the interfaces of both the as-solution and sub-aging specimens exhibit an obvious bonding effecting zone. After the solid-state diffusion bonding and the standard heat treatment, the second γʹ phases in the as-forged specimens are fine, uniform, and spherical. However, the second γʹ phases in the as-solution and sub-aging specimens grow up and split up because of the solid-state diffusion bonding thermal cycle. Different morphology of the second γʹ phases causes the difference of properties in the bonding interface regions. Results of the electron backscattered diffraction (EBSD) show that the preferred orientation of large grains is {100}, and the grain orientation is more obvious as the closer distance to the solid diffusion interface. The tensile test results show that the strength at the interfaces of the forged specimens after the solid-state diffusion bonding and the standard heat treatment is more than 99% of that of the matrix. The tensile cracks mainly initialize from the aggregated area of the large grains and the coarse γʹ phases, which show the transgranular dimple fracture behavior.
format Article
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institution Kabale University
issn 1001-3784
language zho
publishDate 2021-08-01
publisher Editorial Office of Powder Metallurgy Technology
record_format Article
series Fenmo yejin jishu
spelling doaj-art-02b49d3cda4b436eaaaf7625ebf0fca12024-12-12T03:13:27ZzhoEditorial Office of Powder Metallurgy TechnologyFenmo yejin jishu1001-37842021-08-0139431131810.19591/j.cnki.cn11-1974/tf.2021040005Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interfaceYANG Jie0LIU Guang-xu1ZHANG Jing2WANG Wen-ying3WANG Xiao-feng4ZOU Jin-wen5Science and Technology on Advanced High Temperature Structural Materials Laboratory, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaScience and Technology on Advanced High Temperature Structural Materials Laboratory, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaScience and Technology on Advanced High Temperature Structural Materials Laboratory, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaScience and Technology on Advanced High Temperature Structural Materials Laboratory, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaScience and Technology on Advanced High Temperature Structural Materials Laboratory, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaScience and Technology on Advanced High Temperature Structural Materials Laboratory, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, ChinaThe microstructure on the solid-state diffusion bonding interfaces of the initially as-forged, as-solution, and sub-aging FGH96 was characterized, the tensile properties of the bonding interfaces were tested, and the failure behavior was studied. It is found that the good metallurgical bonding is achieved at the bonding interfaces of all the three primitive state specimens after the solid-state diffusion, and no cracks and cavities are found. The interfaces of the as-forged specimens show more sufficient diffusion of elements and smoother transition of microstructure, while the interfaces of both the as-solution and sub-aging specimens exhibit an obvious bonding effecting zone. After the solid-state diffusion bonding and the standard heat treatment, the second γʹ phases in the as-forged specimens are fine, uniform, and spherical. However, the second γʹ phases in the as-solution and sub-aging specimens grow up and split up because of the solid-state diffusion bonding thermal cycle. Different morphology of the second γʹ phases causes the difference of properties in the bonding interface regions. Results of the electron backscattered diffraction (EBSD) show that the preferred orientation of large grains is {100}, and the grain orientation is more obvious as the closer distance to the solid diffusion interface. The tensile test results show that the strength at the interfaces of the forged specimens after the solid-state diffusion bonding and the standard heat treatment is more than 99% of that of the matrix. The tensile cracks mainly initialize from the aggregated area of the large grains and the coarse γʹ phases, which show the transgranular dimple fracture behavior.https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2021040005fgh96 superallysolid-state diffusion bondingmicrostructurefailure mechanism
spellingShingle YANG Jie
LIU Guang-xu
ZHANG Jing
WANG Wen-ying
WANG Xiao-feng
ZOU Jin-wen
Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interface
Fenmo yejin jishu
fgh96 superally
solid-state diffusion bonding
microstructure
failure mechanism
title Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interface
title_full Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interface
title_fullStr Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interface
title_full_unstemmed Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interface
title_short Microstructure and failure mechanism of FGH96 solid-state diffusion bonding interface
title_sort microstructure and failure mechanism of fgh96 solid state diffusion bonding interface
topic fgh96 superally
solid-state diffusion bonding
microstructure
failure mechanism
url https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2021040005
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