Species Differences in Ezetimibe Glucuronidation

Background: Peclinical and clinical studies have revealed that ezetimibe, an approved cholesterol-absorption inhibitor, is rapidly and extensively metabolized to a more potent metabolite, ezetimibe glucuronide. Since different species are commonly used in the pharmacokinetic and pharmacodynamic stud...

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Main Authors: Shalom Emmanuel, Eric A. Asare, Ting Du, Huan Xie, Dong Liang, Song Gao
Format: Article
Language:English
Published: MDPI AG 2024-10-01
Series:Metabolites
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Online Access:https://www.mdpi.com/2218-1989/14/11/569
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author Shalom Emmanuel
Eric A. Asare
Ting Du
Huan Xie
Dong Liang
Song Gao
author_facet Shalom Emmanuel
Eric A. Asare
Ting Du
Huan Xie
Dong Liang
Song Gao
author_sort Shalom Emmanuel
collection DOAJ
description Background: Peclinical and clinical studies have revealed that ezetimibe, an approved cholesterol-absorption inhibitor, is rapidly and extensively metabolized to a more potent metabolite, ezetimibe glucuronide. Since different species are commonly used in the pharmacokinetic and pharmacodynamic studies of ezetimibe, it is essential to determine the species difference in glucuronidation of ezetimibe in order to accurately evaluate ezetimibe’s pharmacokinetics and pharmacodynamics. The purpose of the study was to compare species differences in ezetimibe glucuronidation rates using intestinal microsomes from humans, rats, mice, monkeys, and dogs. Method: Intestinal microsomes from different species were used to assess the ezetimibe glucuronidation rates. Multiple substrate concentrations at 0.5, 2, 5, 10, 20, 30, 40, and 50 µM were tested and fitted into the Michaelis–Menten model to determine the enzyme kinetic parameters. Results: The results showed that the glucuronidation rates with these tested species were significantly different. Kinetic studies revealed that the maximum metabolic rate (V<sub>max</sub>) was higher in monkeys (3.87 ± 0.22 nmol/mg/min) than that in rat (2.40 ± 0.148 nmol/mg/min) and mouse (2.23 ± 0.10 nmol/mg/min), and then human (1.90 ± 0.08 nmol/mg/min) and dog (1.19 ± 0.06 nmol/mg/min). The CLint was an 8.17-fold difference among these species, following the order of mouse > dog > human > rat = monkey. Conclusions: The study revealed that the rate of ezetimibe glucuronidation in the intestine was different in different species and has an impact on ezetimibe glucuronidation in the intestine. When analyzing the pharmacodynamics, pharmacokinetics, or toxicology of ezetimibe using different models, these species differences must be taken into consideration.
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spelling doaj-art-011887deb54d4e299f943bee350d212e2025-08-20T01:54:03ZengMDPI AGMetabolites2218-19892024-10-01141156910.3390/metabo14110569Species Differences in Ezetimibe GlucuronidationShalom Emmanuel0Eric A. Asare1Ting Du2Huan Xie3Dong Liang4Song Gao5Department of Pharmaceutical Science, College of Pharmacy and Health Sciences, Texas Southern University, 3100 Cleburne Street, Houston, TX 77004, USADepartment of Pharmaceutical Science, College of Pharmacy and Health Sciences, Texas Southern University, 3100 Cleburne Street, Houston, TX 77004, USADepartment of Pharmaceutical Science, College of Pharmacy and Health Sciences, Texas Southern University, 3100 Cleburne Street, Houston, TX 77004, USADepartment of Pharmaceutical Science, College of Pharmacy and Health Sciences, Texas Southern University, 3100 Cleburne Street, Houston, TX 77004, USADepartment of Pharmaceutical Science, College of Pharmacy and Health Sciences, Texas Southern University, 3100 Cleburne Street, Houston, TX 77004, USADepartment of Pharmaceutical Science, College of Pharmacy and Health Sciences, Texas Southern University, 3100 Cleburne Street, Houston, TX 77004, USABackground: Peclinical and clinical studies have revealed that ezetimibe, an approved cholesterol-absorption inhibitor, is rapidly and extensively metabolized to a more potent metabolite, ezetimibe glucuronide. Since different species are commonly used in the pharmacokinetic and pharmacodynamic studies of ezetimibe, it is essential to determine the species difference in glucuronidation of ezetimibe in order to accurately evaluate ezetimibe’s pharmacokinetics and pharmacodynamics. The purpose of the study was to compare species differences in ezetimibe glucuronidation rates using intestinal microsomes from humans, rats, mice, monkeys, and dogs. Method: Intestinal microsomes from different species were used to assess the ezetimibe glucuronidation rates. Multiple substrate concentrations at 0.5, 2, 5, 10, 20, 30, 40, and 50 µM were tested and fitted into the Michaelis–Menten model to determine the enzyme kinetic parameters. Results: The results showed that the glucuronidation rates with these tested species were significantly different. Kinetic studies revealed that the maximum metabolic rate (V<sub>max</sub>) was higher in monkeys (3.87 ± 0.22 nmol/mg/min) than that in rat (2.40 ± 0.148 nmol/mg/min) and mouse (2.23 ± 0.10 nmol/mg/min), and then human (1.90 ± 0.08 nmol/mg/min) and dog (1.19 ± 0.06 nmol/mg/min). The CLint was an 8.17-fold difference among these species, following the order of mouse > dog > human > rat = monkey. Conclusions: The study revealed that the rate of ezetimibe glucuronidation in the intestine was different in different species and has an impact on ezetimibe glucuronidation in the intestine. When analyzing the pharmacodynamics, pharmacokinetics, or toxicology of ezetimibe using different models, these species differences must be taken into consideration.https://www.mdpi.com/2218-1989/14/11/569ezetimibeglucuronidationspecies differencesUGT
spellingShingle Shalom Emmanuel
Eric A. Asare
Ting Du
Huan Xie
Dong Liang
Song Gao
Species Differences in Ezetimibe Glucuronidation
Metabolites
ezetimibe
glucuronidation
species differences
UGT
title Species Differences in Ezetimibe Glucuronidation
title_full Species Differences in Ezetimibe Glucuronidation
title_fullStr Species Differences in Ezetimibe Glucuronidation
title_full_unstemmed Species Differences in Ezetimibe Glucuronidation
title_short Species Differences in Ezetimibe Glucuronidation
title_sort species differences in ezetimibe glucuronidation
topic ezetimibe
glucuronidation
species differences
UGT
url https://www.mdpi.com/2218-1989/14/11/569
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AT tingdu speciesdifferencesinezetimibeglucuronidation
AT huanxie speciesdifferencesinezetimibeglucuronidation
AT dongliang speciesdifferencesinezetimibeglucuronidation
AT songgao speciesdifferencesinezetimibeglucuronidation