Synthesis of Polyfunctionalized 4H-Pyrans

Amberlyst A21 catalyzed one-pot three-component coupling of aldehyde and malononitrile with active methylene compounds such as acetylacetone and ethyl acetoacetate for the synthesis of pharmaceutically important polyfunctionalized 4H-pyrans has been reported. Simple experimental procedure, no chroma...

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Main Authors: Manisha Bihani, Pranjal P. Bora, Ghanashyam Bez
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2013/785930
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author Manisha Bihani
Pranjal P. Bora
Ghanashyam Bez
author_facet Manisha Bihani
Pranjal P. Bora
Ghanashyam Bez
author_sort Manisha Bihani
collection DOAJ
description Amberlyst A21 catalyzed one-pot three-component coupling of aldehyde and malononitrile with active methylene compounds such as acetylacetone and ethyl acetoacetate for the synthesis of pharmaceutically important polyfunctionalized 4H-pyrans has been reported. Simple experimental procedure, no chromatographic purification, no hazardous organic solvents, easy recovery and reusability of the catalyst, and room temperature reaction conditions are some of the highlights of this protocol for the synthesis of pharmaceutically relevant focused libraries.
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spelling doaj-art-00660c9d27e44beb90be352aee19fa462025-08-20T02:03:12ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/785930785930Synthesis of Polyfunctionalized 4H-PyransManisha Bihani0Pranjal P. Bora1Ghanashyam Bez2Department of Chemistry, North Eastern Hill University, Shillong 793022, IndiaDepartment of Chemistry, North Eastern Hill University, Shillong 793022, IndiaDepartment of Chemistry, North Eastern Hill University, Shillong 793022, IndiaAmberlyst A21 catalyzed one-pot three-component coupling of aldehyde and malononitrile with active methylene compounds such as acetylacetone and ethyl acetoacetate for the synthesis of pharmaceutically important polyfunctionalized 4H-pyrans has been reported. Simple experimental procedure, no chromatographic purification, no hazardous organic solvents, easy recovery and reusability of the catalyst, and room temperature reaction conditions are some of the highlights of this protocol for the synthesis of pharmaceutically relevant focused libraries.http://dx.doi.org/10.1155/2013/785930
spellingShingle Manisha Bihani
Pranjal P. Bora
Ghanashyam Bez
Synthesis of Polyfunctionalized 4H-Pyrans
Journal of Chemistry
title Synthesis of Polyfunctionalized 4H-Pyrans
title_full Synthesis of Polyfunctionalized 4H-Pyrans
title_fullStr Synthesis of Polyfunctionalized 4H-Pyrans
title_full_unstemmed Synthesis of Polyfunctionalized 4H-Pyrans
title_short Synthesis of Polyfunctionalized 4H-Pyrans
title_sort synthesis of polyfunctionalized 4h pyrans
url http://dx.doi.org/10.1155/2013/785930
work_keys_str_mv AT manishabihani synthesisofpolyfunctionalized4hpyrans
AT pranjalpbora synthesisofpolyfunctionalized4hpyrans
AT ghanashyambez synthesisofpolyfunctionalized4hpyrans