Crystal structure and Hirshfeld surface analysis of (2,7-diethoxynaphthalene-1,8-diyl)bis[(4-bromophenyl)methanone]

The title compound, C28H22Br2O4, crystallizes in the monoclinic space group P21/c at 193 K. The two 4-bromobenzoyl groups are attached in a non-coplanar fashion to the naphthalene ring system and are oriented in opposite directions. The two 4-bromobenzene rings are tilted almost symmetrically with r...

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Bibliographic Details
Main Authors: Kun Li, Jiali Yao, Hiroaki Iitsuka, Noriyuki Yonezawa, Akiko Okamoto
Format: Article
Language:English
Published: International Union of Crystallography 2024-12-01
Series:Acta Crystallographica Section E: Crystallographic Communications
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Online Access:https://journals.iucr.org/paper?S205698902401123X
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Summary:The title compound, C28H22Br2O4, crystallizes in the monoclinic space group P21/c at 193 K. The two 4-bromobenzoyl groups are attached in a non-coplanar fashion to the naphthalene ring system and are oriented in opposite directions. The two 4-bromobenzene rings are tilted almost symmetrically with respect to the naphthalene ring system. The crystal packing features several kinds of non-classical hydrogen bonds such as C—H...X (X = polar atom), in which the C—H group acts as a hydrogen-atom donor, and C—H...π interactions. The two-dimensional fingerprint plots generated in a Hirshfeld surface analysis show non-classical hydrogen bonding with short contacts involving the bromo group.
ISSN:2056-9890