Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharides

As has been confirmed in our previous study, red onion is a promising source of inulin-fructan, inulin neoseries fructan, and their fructooligosaccharides (FOSs). Short-chain FOSs (SCFOSs) are potential prebiotics as they provide many health promoting benefits. However, short-chain inulin neoseries...

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Main Authors: Jirat Wongsanittayarak, Nalapat Leangnim, Kridsada Unban, Chartchai Khanongnuch, Saisamorn Lumyong, Pairote Wongputtisin, Apinun Kanpiengjai
Format: Article
Language:English
Published: Elsevier 2024-12-01
Series:Journal of Agriculture and Food Research
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Online Access:http://www.sciencedirect.com/science/article/pii/S2666154324003909
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author Jirat Wongsanittayarak
Nalapat Leangnim
Kridsada Unban
Chartchai Khanongnuch
Saisamorn Lumyong
Pairote Wongputtisin
Apinun Kanpiengjai
author_facet Jirat Wongsanittayarak
Nalapat Leangnim
Kridsada Unban
Chartchai Khanongnuch
Saisamorn Lumyong
Pairote Wongputtisin
Apinun Kanpiengjai
author_sort Jirat Wongsanittayarak
collection DOAJ
description As has been confirmed in our previous study, red onion is a promising source of inulin-fructan, inulin neoseries fructan, and their fructooligosaccharides (FOSs). Short-chain FOSs (SCFOSs) are potential prebiotics as they provide many health promoting benefits. However, short-chain inulin neoseries oligosaccharides isolated from plants have scarcely been studied. After prebiotic production, a purification step is essential to produce a functional prebiotic. The aim of this study was to develop new processes of integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of SCFOSs. Endo-inulinase is a key enzyme for hydrolysis of crude red onion extract to produce SCFOSs, while Candida orthopsilosis FLA44.2 was employed for purification of the produced SCFOSs. Three different strategies, including two-step (TSP), simultaneous (SP), and semi-simultaneous (SSP) production processes, were designed and investigated as potentially simple, cost-effective, and timesaving production processes. The SP and SSP processes met the objective criteria by exhibiting desirable yields of SCFOSs and the optimal purity of SCFOSs when compared with the TSP process. Notably, the SP process was highlighted as it was simpler than the SSP process. Under optimal conditions (0.4 U of endo-inulinase/g total fructans, 5 % v/v of yeast inoculum and reaction time of 72 h), the SP process conducted in 1-dm3 flasks produced SCFOSs of 87 g/dm3 with neo-GF2 as the main constituent (42 g/dm3) and a purity of 100 %. The ratio of total SCFOSs to total fructans was 0.93 indicating that fructans of the red onion extract have been transformed to SCFOSs.
format Article
id doaj-art-591b433b559f404aaf4916abe2b04736
institution Kabale University
issn 2666-1543
language English
publishDate 2024-12-01
publisher Elsevier
record_format Article
series Journal of Agriculture and Food Research
spelling doaj-art-591b433b559f404aaf4916abe2b047362024-12-16T05:37:29ZengElsevierJournal of Agriculture and Food Research2666-15432024-12-0118101353Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharidesJirat Wongsanittayarak0Nalapat Leangnim1Kridsada Unban2Chartchai Khanongnuch3Saisamorn Lumyong4Pairote Wongputtisin5Apinun Kanpiengjai6Program in Biotechnology, Multidisciplinary and Interdisciplinary School, Chiang Mai University, Chiang Mai, 50200, Thailand; Division of Biochemistry and Biochemical Innovation, Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, ThailandDivision of Biochemistry and Biochemical Innovation, Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand; Office of Research Administration, Chiang Mai University, Chiang Mai, 50200, ThailandDivision of Food Science and Technology, Faculty of Agro-Industry, Chiang Mai University, Chiang Mai, 50100, ThailandDepartment of Biology, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, ThailandDepartment of Biology, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand; Academy of Science, The Royal Society of Thailand, Bangkok, 10300, ThailandProgram in Biotechnology, Faculty of Science, Maejo University, Chiang Mai, 50290, ThailandDivision of Biochemistry and Biochemical Innovation, Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand; Corresponding author.As has been confirmed in our previous study, red onion is a promising source of inulin-fructan, inulin neoseries fructan, and their fructooligosaccharides (FOSs). Short-chain FOSs (SCFOSs) are potential prebiotics as they provide many health promoting benefits. However, short-chain inulin neoseries oligosaccharides isolated from plants have scarcely been studied. After prebiotic production, a purification step is essential to produce a functional prebiotic. The aim of this study was to develop new processes of integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of SCFOSs. Endo-inulinase is a key enzyme for hydrolysis of crude red onion extract to produce SCFOSs, while Candida orthopsilosis FLA44.2 was employed for purification of the produced SCFOSs. Three different strategies, including two-step (TSP), simultaneous (SP), and semi-simultaneous (SSP) production processes, were designed and investigated as potentially simple, cost-effective, and timesaving production processes. The SP and SSP processes met the objective criteria by exhibiting desirable yields of SCFOSs and the optimal purity of SCFOSs when compared with the TSP process. Notably, the SP process was highlighted as it was simpler than the SSP process. Under optimal conditions (0.4 U of endo-inulinase/g total fructans, 5 % v/v of yeast inoculum and reaction time of 72 h), the SP process conducted in 1-dm3 flasks produced SCFOSs of 87 g/dm3 with neo-GF2 as the main constituent (42 g/dm3) and a purity of 100 %. The ratio of total SCFOSs to total fructans was 0.93 indicating that fructans of the red onion extract have been transformed to SCFOSs.http://www.sciencedirect.com/science/article/pii/S2666154324003909Red onionFructooligosaccharidesNeofructooliogsaccharidesNeokestoseEndo-inulinaseYeast treatment
spellingShingle Jirat Wongsanittayarak
Nalapat Leangnim
Kridsada Unban
Chartchai Khanongnuch
Saisamorn Lumyong
Pairote Wongputtisin
Apinun Kanpiengjai
Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharides
Journal of Agriculture and Food Research
Red onion
Fructooligosaccharides
Neofructooliogsaccharides
Neokestose
Endo-inulinase
Yeast treatment
title Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharides
title_full Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharides
title_fullStr Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharides
title_full_unstemmed Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharides
title_short Integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short-chain inulin and inulin neoseries oligosaccharides
title_sort integrated enzymatic hydrolysis of crude red onion extract and yeast treatment for production and purification of short chain inulin and inulin neoseries oligosaccharides
topic Red onion
Fructooligosaccharides
Neofructooliogsaccharides
Neokestose
Endo-inulinase
Yeast treatment
url http://www.sciencedirect.com/science/article/pii/S2666154324003909
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